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Vol. 35 No. 2 (2023): Vol 35 Issue 2, 2023

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Hydrothermal Synthesis of In2O3-SiO2 as Recyclable Mesostructured Catalyst Utilized for 2,3-Dihydrophthalazine-1,4-dione (DHP) Derivatives

https://doi.org/10.14233/ajchem.2023.24060
D. Tayde
Department of Chemistry, M.J.M. Arts, Commerce and Science College, Karanjali-422208, India
U. Gawai
Department of Chemistry, Late Annasaheb R.D. Deore Arts and Science College, Mhasadi-424304, India
R. Nikam
Department of Chemistry, M.J.M. Arts, Commerce and Science College, Karanjali-422208, India
V. Ingale
Department of Chemistry, Arts, Commerce College, Warvat Bakal-444202, India
M. Lande
Department of Chemistry, Dr. Babasaheb Ambedkar Marathwada University, Aurangabad-431004, India

Corresponding Author(s) : D. Tayde

dtt_chem@yahoo.com

Asian Journal of Chemistry, Vol. 35 No. 2 (2023): Vol 35 Issue 2, 2023

Abstract

Mesostructured In2O3-SiO2 as recyclable heterogeneous catalyst material was synthesized by an aqueous solution based wet chemistry method, i.e. hydrothermal method and utilized for the reaction between pathalic anhydride and substituted hydrazine hydrate in DMF medium to synthesize 2,3-dihydrophthalazine-1,4-dione (DHP) derivatives. The advantages of this protocol are cost effective, ease of handling and environmental friendly. This catalytic material were characterized by using X-ray diffraction spectroscopy, scanning electron microscopy, energy dispersive spectroscopy, Fourier transform infrared spectroscopy, temperature-programmed desorption and Brunauer–Emmett–Teller. The proposed synthetic method results in a high yield, has an easy work-up procedure, is non-toxic and clean, and facilitates the simple recovery and reusability of the catalytic system.

Keywords

Mesostructured Reusability Hydrothermal method Phthalzine-1,4-diones
Tayde, D., Gawai, U., Nikam, R., Ingale, V., & Lande, M. (2023). Hydrothermal Synthesis of In2O3-SiO2 as Recyclable Mesostructured Catalyst Utilized for 2,3-Dihydrophthalazine-1,4-dione (DHP) Derivatives. Asian Journal of Chemistry, 35(2), 507–512. https://doi.org/10.14233/ajchem.2023.24060
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