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Vol. 34 No. 12 (2022): Vol 34 Issue 12, 2022

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Determination of Concentration of Various Phases in Activated and Dye Treated Sewage Sludge Samples using Synchrotron X-Ray Diffraction

https://doi.org/10.14233/ajchem.2022.23945
Priyanka Shrivastava
Department of Chemistry, Government Holkar (Model Autonomous) Science College, Indore-452017, India
Vibha Malviya
Department of Chemistry, Government Holkar (Model Autonomous) Science College, Indore-452017, India
Anjali Yadav
Department of Chemistry, Government Holkar (Model Autonomous) Science College, Indore-452017, India
Payal Jain
Department of Chemistry, Government Holkar (Model Autonomous) Science College, Indore-452017, India
Ruchika Malviya
Department of Chemistry, Government Holkar (Model Autonomous) Science College, Indore-452017, India
M.K. Dwivedi
Department of Chemistry, Government Holkar (Model Autonomous) Science College, Indore-452017, India
A.K. Sinha
HXAL, Synchrotron Utilization Section, Raja Ramanna Centre for Advanced Technology, Indore-452013, India

Corresponding Author(s) : M.K. Dwivedi

dwivedimk12@gmail.com

Asian Journal of Chemistry, Vol. 34 No. 12 (2022): Vol 34 Issue 12, 2022

Abstract

Sludge sample collected from sewage treatment plant was used to develop an effective adsorbent for the removal of various dyes from wastewater. A quantitative estimation of major compounds in without activated (as collected), activated and various dyes treated sludge samples using synchrotron XRD technique is reported. Sewage sludge sample activated at 900 ºC for 30 min was found to have maximum adsorption efficiency (~ 95%) for the removal of different dyes (e.g. brilliant green, crystal violet and malachite green) from aqueous solution. The result shows that the adsorption using activated sewage sludge is the simplest and effective method for the removal of dyes from wastewater. As expected, the major compound in all the samples is SiO2 (~ 50 mol%). However, SiO2 was found in three different space groups. On activation at 900 ºC, a part of monoclinic SiO2 phase changes to the hexagonal phase. On the other hand, on various dyes adsorption such as brilliant green, crystal violet and malachite green, the monoclinic phase changes to the tetragonal phase.

Keywords

Adsorbent Analysis Sludge Synchrotron radiation X-ray diffraction
Shrivastava, P., Malviya, V., Yadav, A., Jain, P., Malviya, R., Dwivedi, M., & Sinha, A. (2022). Determination of Concentration of Various Phases in Activated and Dye Treated Sewage Sludge Samples using Synchrotron X-Ray Diffraction. Asian Journal of Chemistry, 34(12), 3308–3312. https://doi.org/10.14233/ajchem.2022.23945
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