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Magnetically Recoverable Fe0.02Zn0.95-xCr0.05O Iron doped Catalyst for Synthesis of Dihydropyrimidones, Thiones and their Derivatives
Corresponding Author(s) : A.W. Suryawanshi
Asian Journal of Chemistry,
Vol. 34 No. 12 (2022): Vol 34 Issue 12, 2022
Abstract
A new technique for the impregnation of magnetic based catalyst component onto the organic molecules are widely discussed. Due to its benefits of high surface area, separation simplicity, recyclability and limited leaching of catalytic active ingredients from the catalyst, in the present work, iron-doped Fe0.02Zn0.95-xCr0.05O heterogeneous catalyst was applied in the synthesis of dihydropyrimidones, thiones and their derivatives. The synthesized compounds were elucidated by their IR, 1H NMR and 13C NMR and LC-MS analysis.
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- B. Mohammadi and F.K. Behbahani, Mol. Divers., 22, 405 (2018); https://doi.org/10.1007/s11030-017-9806-z
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References
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H.G.O. Alvim, E.N. da Silva Jr. and B.A.D. Neto, RSC Adv., 4, 54282 (2014); https://doi.org/10.1039/C4RA10651B
B. Mohammadi and F.K. Behbahani, Mol. Divers., 22, 405 (2018); https://doi.org/10.1007/s11030-017-9806-z
C.O. Kappe, Acc. Chem. Res., 33, 879 (2000); https://doi.org/10.1021/ar000048h
N. Podilla and T. Choudhury, J. Appl. Pharm. Res., 6, 11 (2018); https://doi.org/10.18231/2348-0335.2018.0003
M. Marinescu, Molecules, 26, 6022 (2021); https://doi.org/10.3390/molecules26196022
J. Rani, S. Kumar, M. Saini, J. Mundlia and P.K. Verma, Res. Chem. Intermed., 42, 6777 (2016); https://doi.org/10.1007/s11164-016-2525-8
R. Kaur, S. Chaudhary, K. Kumar, M.K. Gupta and R.K. Rawal, Eur. J. Med. Chem., 132, 108 (2017); https://doi.org/10.1016/j.ejmech.2017.03.025
H.N. Karade, M. Sathe and M.P. Kaushik, Molecules, 12, 1341 (2007); https://doi.org/10.3390/12071341
A.D. Shutalev, E.A. Kishko, N.V. Sivova and A.Y. Kuznetsov, Molecules, 3, 100 (1998); https://doi.org/10.3390/30300100
S. Ghassamipour and A.R. Sardarian, J. Iranian Chem. Soc., 7, 237 (2010).
Z.-L. Shen and S.-J. Ji, Synth. Commun., 39, 808 (2009); https://doi.org/10.1080/00397910802431172
J.S. Yadav, B.V.S. Reddy, K. Bhaskar Reddy, K. Sarita Raj and A.R. Prasad, J. Chem. Soc., Perkin Trans. 1, 1939 (2001); https://doi.org/10.1039/b102565c
Y. Ma, C. Qian, L. Wang and M. Yang, J. Org. Chem., 65, 3864 (2000); https://doi.org/10.1021/jo9919052
B.C. Ranu, A. Hajra and U. Jana, J. Org. Chem., 65, 6270 (2000); https://doi.org/10.1021/jo000711f
I. Ugi, B. Werner and A. Dömling, Molecules, 8, 53 (2003); https://doi.org/10.3390/80100053
A. Dömling, W. Wang and K. Wang, Chem. Rev., 112, 3083 (2012); https://doi.org/10.1021/cr100233r
F. Sweet and J.D. Fissekis, J. Am. Chem. Soc., 95, 8741 (1973); https://doi.org/10.1021/ja00807a040
K. Folkers and T.B. Johnson, J. Am. Chem. Soc., 55, 3784 (1933); https://doi.org/10.1021/ja01336a054
I. Cepanec, M. Litvic, M. Filipan-Litvic and I. Grüngold, Tetrahedron, 63, 11822 (2007); https://doi.org/10.1016/j.tet.2007.09.045
S. Kalidindi and B. Jagirdar, ChemSusChem, 5, 65 (2012); https://doi.org/10.1002/cssc.201100377
A. Marandi, N. Koukabi and M.A. Zolfigol, Res. Chem. Intermed., 47, 3145 (2021); https://doi.org/10.1007/s11164-021-04457-z
A. Maleki, Z. Hajizadeh and R. Firouzi-Haji, Micropor. Mesopor. Mater., 259, 46 (2018); https://doi.org/10.1016/j.micromeso.2017.09.034
Z.B. Shifrina and L.M. Bronstein, Front. Chem., 6, 298 (2018); https://doi.org/10.3389/fchem.2018.00298
A. Ashok, T. Ratnaji, L.J. Kennedy, J.J. Vijaya and R.G. Pragash, Renew. Energy, 163, 480 (2021); https://doi.org/10.1016/j.renene.2020.08.081
X. Zhang, M.A. Ashraf, Z. Liu and D. Zhang, Synth. Commun., 50, 2705 (2020); https://doi.org/10.1080/00397911.2020.1785504
S. Balsure, M. Gurav, R. Kadam, K. Haval, R. Tigote and A. Kadam, Ceramica, 68, 24 (2022); https://doi.org/10.1590/0366-69132022683853187
K. Akhter, K. Jahan, U.K.R. Romman, M.G. Ahmed, M.S. Rahman and M. Al-Amin, Asian J. Chem., 27, 2624 (2015); https://doi.org/10.14233/ajchem.2015.18615
S. Chancharunee, P. Pinhom, M. Pohmakotr and P. Perlmutter, Synth. Commun., 39, 880 (2009); https://doi.org/10.1080/00397910802439175
X. Han, F. Xu, Y. Luo and Q. Shen, Eur. J. Org. Chem., 1500 (2005); https://doi.org/10.1002/ejoc.200400753