Hyphenated GC-MS Determination of Volatile Constituents in Lilium

Xiaojing Wang; Yueming Yu; Sufen Guo

doi:10.14233/ajchem.2014.15604

Issue

Vol. 26 No. 7 (2014): Vol 26 Issue 7

Issue Published : March 22, 2014

This work is licensed under a Creative Commons Attribution 4.0 International License.

Hyphenated GC-MS Determination of Volatile Constituents in Lilium

https://doi.org/10.14233/ajchem.2014.15604

Xiaojing Wang

School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, P.R. China

Yueming Yu

School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, P.R. China

Sufen Guo

Tianjin Pharmaceutical Design Institute, Tianjin 300040, P.R. China

Corresponding Author(s) : Xiaojing Wang

tdxjwang@163.com

Asian Journal of Chemistry, Vol. 26 No. 7 (2014): Vol 26 Issue 7
Article Published : March 31, 2014

Abstract

Volatile components of lilium were extracted by water steam distillation and analyzed by using gas chromatography-mass spectrometry (GC-MS). A total of 72 volatile oil components were identified and the relative content of each component was determined by area normalization. Among 72 volatile oil components, 48 compounds identified amount to 77.28 % of the total amount of volatile oil. The major compounds were found to be 1-dodecene (8.04 %), 1-docosene (7.35 %), 1-hexadecanol (5 %), ethanol, 2-(9-octadecenyloxy)-, (Z)- (4.22%), n-hexadecanoic acid (3.27 %), benzofuran, 4,7-dimethyl- (3.26%) and hexadecane-1,2-diol (3.09 %).

Keywords

Lilium Volatile oil Water steam distillation Gas chromatography-mass spectrometry

Wang, X., Yu, Y., & Guo, S. (2014). Hyphenated GC-MS Determination of Volatile Constituents in Lilium. Asian Journal of Chemistry, 26(7), 1974–1976. https://doi.org/10.14233/ajchem.2014.15604

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Pharmacopoeia of PRC, Chemistry Industry Press, p. 88 (2005).

Y. Mimaki, O. Nakamura, Y. Sashida, Y. Satomi, A. Nishino and H. Nishino, Phytochemistry, 37, 227 (1994); doi:10.1016/0031-9422(94)85030-5.

A. Brossi, J. Med. Chem., 33, 2311 (1990); doi:10.1021/jm00171a001.

H. Shimomura, Y. Sashida and Y. Mimaki, Phytochemistry, 25, 2897 (1986); doi:10.1016/S0031-9422(00)83765-6.

H. Shimomura, Y. Sashida, Y. Mimaki and N. Iida, Phytochemistry, 27, 451 (1988); doi:10.1016/0031-9422(88)83118-2.

Y. Mimaki, N. Ishibashi, K. Ori and Y. Sashida, Phytochemistry, 31, 1753 (1992); doi:10.1016/0031-9422(92)83141-K.

K. Nakano, K. Nishizawa, I. Takemoto, K. Murakami, Y. Takaishi and T. Tomimatsu, Phytochemistry, 27, 1897 (1988); doi:10.1016/0031-9422(88)80476-X.

T. Satou, Y. Mimaki, M. Kuroda, Y. Sashida and Y. Hatakeyama, Phytochemistry, 41, 1225 (1996); doi:10.1016/0031-9422(95)00723-7.

J.A. Francis, B. Rumbeiha and M.G. Nair, Life Sci., 76, 671 (2004); doi:10.1016/j.lfs.2004.10.001.

J.P. Munafo Jr. and T.J. Gianfagna, J. Agric. Food Chem., 59, 995 (2011); doi:10.1021/jf1036454.

Y. Mimaki, T. Satou, M. Kuroda, Y. Sashida and Y. Hatakeyama, Phytochemistry, 51, 567 (1999); doi:10.1016/S0031-9422(99)00022-9.

X.W. Yang, Y.S. Wu, Y.X. Cui, X.H. Liu and S.Y. Xiao, Acta Pharmacol. Sin., 37, 863 (2002).

E. Eisenreichová, M. Haladová, A. Bučková, J. Tomko, D. Uhrín and K. Ubik, Phytochemistry, 31, 1084 (1992).

I. Masterova, D. Uhrin and J. Tomko, Phytochemistry, 26, 1844 (1987); doi:10.1016/S0031-9422(00)82304-3.

H. Kameoka, Dev. Food Sci., 18, 469 (1988).

I. Toyomasa, O. Masanori and N. Hideo, Koryo, Terupen oyobi Seiyu Kagaku ni kansuru Toronkai Koen Yoshishu, 42, 30 (1998) (in Japanese).

P. Lin, J. Cai, J. Li, W.Q. Sang and Q.D. Su, Flav. Fragr. J., 18, 539 (2003); doi:10.1002/ffj.1264.

H. Farsam, M. Amanlou, G. Amin, G. Nezamivand-Chegini, M.H. Salehi-Surmaghi and A. Shafiee, J. Pharm. Sci., 11, 164 (2003).

H.J. Li, L.X. Niu and Z.N. Li, J. Northwest Sci-Tech Univ. Agric. Forestry, 35, 149 (2007).

D.D. Roberts, P. Pollien and C. Milo, J. Agric. Food Chem., 48, 2430 (2000); doi:10.1021/jf991116l.

L. Mondello, R. Costa, P.Q. Tranchida, B. Chiofalo, A. Zumbo, P. Dugo and G. Dugo, Flav. Fragr. J., 20, 659 (2005); doi:10.1002/ffj.1529.

N. Natali, F. Chinnici and C. Riponi, J. Agric. Food Chem., 54, 8190 (2006); doi:10.1021/jf0614387.

S.J. Lee and B. Ahn, Food Chem., 114, 600 (2009); doi:10.1016/j.foodchem.2008.09.091.

Issue

Vol. 26 No. 7 (2014): Vol 26 Issue 7

Hyphenated GC-MS Determination of Volatile Constituents in Lilium

Corresponding Author(s) : Xiaojing Wang

Abstract

Keywords

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