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Vol. 26 No. 6 (2014): Vol 26 Issue 6

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Preparation and Characterization of Ag-MWO4/Zeolite (M = Fe, Ni) Composites by Cyclic Microwave-Assisted Metathetic Method

https://doi.org/10.14233/ajchem.2014.15831B
Chang Sung Lim
Department of Advanced Materials Science & Engineering, Hanseo University, Seosan 356-706, Republic of Korea

Corresponding Author(s) : Chang Sung Lim

cslim@hanseo.ac.kr

Asian Journal of Chemistry, Vol. 26 No. 6 (2014): Vol 26 Issue 6

Abstract

Ag-MWO4/zeolite (M = Fe, Ni) composites were successfully synthesized by a cyclic microwave-assisted metathetic route followed by heat treatment. The characteristics of the exothermic reaction accompanying the by-product of NaCl were found to drive the microwave-assisted metathetic reaction for Wolframite-type FeWO4 and NiWO4 toward completion. The Ag-MWO4/zeolite (M = Fe, Ni) composites were formed completely at 600 ºC. Monoclinic-like crystals of FeWO4 and NiWO4 were primarily co-mixed with porous zeolite-A. Small spherical silver particles were well immobilized in the MWO4/zeolite (M = Fe, Ni) matrix.

Keywords

Cyclic MAM synthesis Ag-MWO4/zeolite (M = Fe Ni) composites Microstructure Immobilization
Sung Lim, C. (2014). Preparation and Characterization of Ag-MWO4/Zeolite (M = Fe, Ni) Composites by Cyclic Microwave-Assisted Metathetic Method. Asian Journal of Chemistry, 26(6), 1853–1856. https://doi.org/10.14233/ajchem.2014.15831B
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