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Vol. 26 No. 6 (2014): Vol 26 Issue 6

Copyright (c) 2014 AJC

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Cyclic Microwave-Assisted Metathetic Synthesis and Spectroscopic Properties of SPION/SrWO4:Er3+, Yb3+ Composites

https://doi.org/10.14233/ajchem.2014.16403
Chang Sung Lim
Department of Advanced Materials Science & Engineering, Hanseo University, Seosan 356-706, Republic of Korea

Corresponding Author(s) : Chang Sung Lim

cslim@hanseo.ac.kr

Asian Journal of Chemistry, Vol. 26 No. 6 (2014): Vol 26 Issue 6

Abstract

Er3+/Yb3+ co-doped SrWO4(SrWO4:Er3+/Yb3+) composites with superparamagnetic iron oxide nanoparticles (SPIONs) were successfully synthesized by a cyclic microwave-assisted metathetic method followed by heat-treatment. The microstructure exhibited well-defined and homogeneous morphology with the SrWO4:Er3+/Yb3+ particle size of 1-2 μm and Fe3O4 particle size of 0.1-0.5 μm. The Fe3O4 particles were self-preferentially crystallized and immobilized on the surface of SrWO4:Er3+/Yb3+ particles. The synthesized SPION/SrWO4:Er3+/Yb3+ composites were characterized by X-ray diffraction, scanning electron microscopy and energy-dispersive X-ray spectroscopy. Other spectroscopic properties were also examined using photoluminescence emission measurements and Raman spectroscopy.

Keywords

SPIONs SrWO4:Er3 /Yb3 Microwave-assisted metathetic synthesis SEM EDX Raman spectroscopy
Sung Lim, C. (2014). Cyclic Microwave-Assisted Metathetic Synthesis and Spectroscopic Properties of SPION/SrWO4:Er3+, Yb3+ Composites. Asian Journal of Chemistry, 26(6), 1848–1852. https://doi.org/10.14233/ajchem.2014.16403
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