Synthesis and Spectroscopic Properties of Superparamagnetic Iron Oxide Nanoparticle/CaWO4:Er3+, Yb3+ Composites by Microwave-Assisted Metathetic Method

Chang Sung Lim

doi:10.14233/ajchem.2014.17213

Issue

Vol. 26 No. 5 (2014): Vol 26 Issue 5

Issue Published : March 1, 2014

This work is licensed under a Creative Commons Attribution 4.0 International License.

Synthesis and Spectroscopic Properties of Superparamagnetic Iron Oxide Nanoparticle/CaWO4:Er3+, Yb3+ Composites by Microwave-Assisted Metathetic Method

https://doi.org/10.14233/ajchem.2014.17213

Chang Sung Lim

Department of Advanced Materials Science & Engineering, Hanseo University, Seosan 356-706, Republic of Korea

Corresponding Author(s) : Chang Sung Lim

cslim@hanseo.ac.kr

Asian Journal of Chemistry, Vol. 26 No. 5 (2014): Vol 26 Issue 5
Article Published : March 3, 2014

Abstract

Er³⁺/Yb³⁺ co-doped CaWO₄(CaWO₄:Er³⁺/Yb³⁺) composites with superparamagnetic iron oxide nanoparticles (SPIONs) were successfully synthesized by a cyclic microwave-assisted metathetic method followed by heat-treatment. The microstructure exhibited well-defined and homogeneous morphology with the CaWO₄:Er³⁺/Yb³⁺ particle size of 1-2 μm and Fe₃O₄ particle size of 0.1-0.5 μm. The Fe₃O₄ particles were self-preferentially crystallized and immobilized on the surface of CaWO₄:Er³⁺/Yb³⁺ particles. The synthesized SPION/CaWO₄:Er³⁺/Yb³⁺ composites were characterized by X-ray diffraction, scanning electron microscopy and energy-dispersive X-ray spectroscopy. Spectroscopic properties were examined using Raman spectroscopy.

Keywords

SPIONs CaWO4:Er3 /Yb3 Microwave-assisted metathetic synthesis SEM/EDS Raman spectroscopy

Sung Lim, C. (2014). Synthesis and Spectroscopic Properties of Superparamagnetic Iron Oxide Nanoparticle/CaWO4:Er3+, Yb3+ Composites by Microwave-Assisted Metathetic Method. Asian Journal of Chemistry, 26(5), 1297–1300. https://doi.org/10.14233/ajchem.2014.17213

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References

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References

D. Liu, L. Tong, J. Shi and H. Yang, J. Alloys Comp., 512, 361 (2012); doi:10.1016/j.jallcom.2011.09.100.

L. Liu, L. Xiao and H.Y. Zhu, Chem. Phys. Lett., 539-540, 112 (2012); doi:10.1016/j.cplett.2012.04.063.

Q. Wang, X. Yang, L. Yu and H. Yang, J. Alloys Comp., 509, 9098 (2011); doi:10.1016/j.jallcom.2011.06.058.

J.H. Ryu, G.S. Park, K.M. Kim, C.S. Lim, J.-W. Yoon and K.B. Shim, Appl. Phys., A Mater. Sci. Process., 88, 731 (2007); doi:10.1007/s00339-007-4051-4.

H. Wu, Y. Hu, F. Kang, L. Chen, X. Wang, G. Ju and Z. Mu, Mater. Res. Bull., 46, 2489 (2011); doi:10.1016/j.materresbull.2011.08.022.

G.H. Lee and S. Kang, J. Lumin., 131, 2606 (2011); doi:10.1016/j.jlumin.2011.06.026.

F.B. Cao, L.S. Li, Y.W. Tian, Y.J. Chen and X.R. Wu, Thin Solid Films, 519, 7971 (2011); doi:10.1016/j.tsf.2011.05.010.

J. Liao, B. Qiu, H. Wen, J. Chen, W. You and L. Liu, J. Alloy. Comp., 487, 758 (2009); doi:10.1016/j.jallcom.2009.08.068.

Y. Zheng, Y. Huang, M. Yang, N. Guo, H. Qiao, Y. Jia and H. You, J. Lumin., 132, 362 (2012); doi:10.1016/j.jlumin.2011.09.010.

M. Sadegh, A. Badiei, A. Abbasi, H. Goldooz and G. Mohammadi Ziarani, J. Lumin., 130, 2072 (2010); doi:10.1016/j.jlumin.2010.05.029.

W. Wang, P. Yang, S. Gai, N. Niu, F. He and J. Lin, J. Nanopart. Res., 12, 2295 (2010); doi:10.1007/s11051-010-9850-4.

Y. Tian, Y. Liu, R. Hua, L. Na and B. Chen, Mater. Res. Bull., 47, 59 (2012); doi:10.1016/j.materresbull.2011.10.007.

C.S. Lim, Mater. Chem. Phys., 131, 714 (2012); doi:10.1016/j.matchemphys.2011.10.039.

C.S. Lim, J. Lumin., 132, 1774 (2012); doi:10.1016/j.jlumin.2012.02.024.

T.T. Basiev, A.A. Sobol, Y.K. Voronko and P.G. Zverev, Opt. Mater., 15, 205 (2000); doi:10.1016/S0925-3467(00)00037-9.

T.T. Basiev, A.A. Sobol, P.G. Zverev, L.I. Ivleva, V.V. Osiko and R.C. Powell, Opt. Mater., 11, 307 (1999); doi:10.1016/S0925-3467(98)00030-5.

D. Rangappa, T. Fujiwara, T. Watanabe and M. Yoshimura, J. Electroceram., 17, 853 (2006); doi:10.1007/s10832-006-0459-z.

V.V. Atuchin, T.A. Gavrilova, V.G. Kostrovsky, L.D. Pokrovsky and I.B. Troitskaia, Inorg. Mater., 44, 622 (2008); doi:10.1134/S0020168508060149.

V.V. Atuchin, O.D. Chimitova, T.A. Gavrilova, M.S. Molokeev, S.J. Kim, N.V. Surovtsev and B.G. Bazarov, J. Cryst. Growth, 318, 683 (2011); doi:10.1016/j.jcrysgro.2010.09.076.

V.V. Atuchin, T.A. Gavrilova, T.I. Grigorieva, N.V. Kuratieva, K.A. Okotrub, N.V. Pervukhina and N.V. Surovtsev, J. Cryst. Growth, 318, 987 (2011); doi:10.1016/j.jcrysgro.2010.10.149.

C.S. Lim, Mater. Res. Bull., 47, 4220 (2012); doi:10.1016/j.materresbull.2012.09.029.

V.V. Atuchin, V.G. Grossman, S.V. Adichtchev, N.V. Surovtsev, T.A. Gavrilova and B.G. Bazarov, Opt. Mater., 34, 812 (2012); doi:10.1016/j.optmat.2011.11.016.

C.S. Lim, Mater. Res. Bull., 48, 3805 (2013); doi:10.1016/j.materresbull.2013.05.090.

C.S. Lim, Mater. Chem. Phys., 140, 154 (2013); doi:10.1016/j.matchemphys.2013.03.014.

Issue

Vol. 26 No. 5 (2014): Vol 26 Issue 5

Synthesis and Spectroscopic Properties of Superparamagnetic Iron Oxide Nanoparticle/CaWO4:Er3+, Yb3+ Composites by Microwave-Assisted Metathetic Method

Corresponding Author(s) : Chang Sung Lim

Abstract

Keywords

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