Determination of (-)-Borneol, Camphor and Isoborneol in Blumea balsamifera (L.) DC. Leaves by Simultaneous Ultrasonic and Microwave Assisted Extraction and Gas Chromatography

Y. Wang; A. Wang; H. Tian; H. Wang; C. Zou

doi:10.14233/ajchem.2014.15737

Issue

Vol. 26 No. 4 (2014): Vol 26 Issue 4

Issue Published : February 15, 2014

This work is licensed under a Creative Commons Attribution 4.0 International License.

Determination of (-)-Borneol, Camphor and Isoborneol in Blumea balsamifera (L.) DC. Leaves by Simultaneous Ultrasonic and Microwave Assisted Extraction and Gas Chromatography

https://doi.org/10.14233/ajchem.2014.15737

Y. Wang

School of Food Science and Technology, State Key Laboratory of Food Science and Technology, Jiangnan University, Wuxi 214122, P.R. China

A. Wang

School of Food Science and Technology, State Key Laboratory of Food Science and Technology, Jiangnan University, Wuxi 214122, P.R. China

H. Tian

School of Food Science and Technology, State Key Laboratory of Food Science and Technology, Jiangnan University, Wuxi 214122, P.R. China

H. Wang

School of Food Science and Technology, State Key Laboratory of Food Science and Technology, Jiangnan University, Wuxi 214122, P.R. China

C. Zou

Gui Zhou Ai Yuan Eco-Pharmaceutical Development Co. Ltd., Luodian 550100, P.R. China

Corresponding Author(s) : H. Wang

xblack1983@eyou.com

Asian Journal of Chemistry, Vol. 26 No. 4 (2014): Vol 26 Issue 4
Article Published : February 14, 2014

Abstract

In present work, simultaneous ultrasonic and microwave assisted extraction followed by GC-FID was developed for quantitative analysis of the bioactive components of (-)-borneol, camphor and isoborneol in Blumea balsamifera leaves. After systematical investigation, the optimal experimental parameters microwave power (100 W) and extraction time (30 s) were investigated. The optimized method provided satisfactory linearity, precision, stability and recovery. The proposed method was applied for determination of three target compounds in leaves samples from 14 different times of harvest period. The variations of three target compounds were monitored and the result demonstrates (-)-borneol content of leaves was higher level from mid-October to next January. It has been shown that the proposed ultrasonic and microwave assisted extraction-GC-FID is a simple, rapid and reliable method for quantitative analysis of (-)-borneol, camphor and isoborneol in B. balsamifera leaves and a potential tool for quality assessment of B. balsamifera leaves.

Keywords

Blumea balsamifera (L.) DC. Leaves Simultaneous ultrasonic and microwave assisted extraction (-)-Borneol

Wang, Y., Wang, A., Tian, H., Wang, H., & Zou, C. (2014). Determination of (-)-Borneol, Camphor and Isoborneol in Blumea balsamifera (L.) DC. Leaves by Simultaneous Ultrasonic and Microwave Assisted Extraction and Gas Chromatography. Asian Journal of Chemistry, 26(4), 997–1001. https://doi.org/10.14233/ajchem.2014.15737

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R. Lin, Flora Republicae Popularis Sinicae, vol. 75, Science Press, Beijing, p. 19-20 (1979).

T.C. Zhu, Y.X. Wen, H.S. Wang and Y.L. Huang, Guihaia, 28, 141 (2008).

M.N.I. Bhuiyan, J.U. Chowdhury and J. Begum, Bangladesh J. Bot., 38, 109 (2009).

Chinese Pharmacopoeia Commission, Pharmacopoeia of The People’s Republic of China, 2010 edition, vol. 1, China Medical Science Press, Beijing, (2010).

Q. Shen, X. Li, W.J. Li and X.Y. Zhao, AAPS PharmSciTech, 12, 1044 (2011);doi: 10.1208/s12249-011-9672-4.

W.R. Li, R.Y. Chen, L. Yang, T.L. Huang, Q.W. Xu, S.Q. Mi and N.-S. Wang, Eur. J. Drug Metab. Pharmacokinet., 37, 39 (2012);doi:10.1007/s13318-011-0058-5.

E. Cherneva, V. Pavlovic, A. Smelcerovic and D. Yancheva, Molecules, 17, 10258 (2012); doi:10.3390/molecules170910258.

J.C. Silva-Filho, N.N.P. M. Oliveira, D.D.R. Arcanjo, L.J. Quintans Jr., S.C.H. Cavalcanti, M.R.V. Santos, R. de Cássia M. Oliveira and A.P. Oliveira, Basic Clin. Pharmacol. Toxicol., 110, 171 (2012); doi:10.1111/j.1742-7843.2011.00784.x.

R. Liu, L. Zhang, X. Lan, L. Li, T.-T. Zhang, J.-H. Sun and G.-H. Du, Neuroscience, 176, 419 (2011); doi:10.1016/j.neuroscience.2010.11.029.

X. Jiang, J. Pan, J. Si and B. Pan, Biomass Chem. Eng., 40, 20 (2006).

K.M. Lee, S.Y. Dai, T.J. Herrman and J.M.B. Musser, J. Chromatogr. B: Analyt. Technol. Biomed. Life Sci., 905, 133 (2012); doi:10.1016/j.jchromb.2012.07.039.

C.H. Deng, Y. Mao, N. Yao and X.M. Zhang, Anal. Chim. Acta, 575, 120 (2006); doi:10.1016/j.aca.2006.05.073.

L. Dong, J.Y. Wang, C.H. Deng and X.Z. Shen, J. Sep. Sci., 30, 86 (2007);doi: 10.1002/jssc.200600207.

Q. Ye and C.H. Deng, Anal. Lett., 41, 2387 (2008);doi:10.1080/00032710802350583.

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X.L. Cheng, J.Y. Wan, P. Li and L.W. Qi, J. Chromatogr. A, 1218, 5774 (2011);doi:10.1016/j.chroma.2011.06.091.

H. Sereshti, Y. Izadmanesh and S. Samadi, J. Chromatogr. A, 1218, 4593 (2011); doi:10.1016/j.chroma.2011.05.037.

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Issue

Vol. 26 No. 4 (2014): Vol 26 Issue 4

Determination of (-)-Borneol, Camphor and Isoborneol in Blumea balsamifera (L.) DC. Leaves by Simultaneous Ultrasonic and Microwave Assisted Extraction and Gas Chromatography

Corresponding Author(s) : H. Wang

Abstract

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