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Vol. 26 No. 3 (2014): Vol 26 Issue 3

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Solvent-Free Synthesis of N-aryl-b-Enaminones Under Microwave Irradiation

https://doi.org/10.14233/ajchem.2014.15524
Guangyong Xie
Key Laboratory of Rubber-Plastics of Ministry of Education/Shandong Provincial Key Laboratory of Rubber -plastics, Qingdao University of Science & Technology, Qingdao 266042, P.R. China ; Key Laboratory of Catalysis and Materials Science of Hubei Province, College of Chemistry and Materials Science, South-Central University for Nationalities, Wuhan 430074, P.R. China ;Ministry of Education Key Laboratory for the Green Preparation and Application of Functional Materials, Hubei University, Wuhan 430062, P.R. China
Long Li
Key Laboratory of Catalysis and Materials Science of Hubei Province, College of Chemistry and Materials Science, South-Central University for Nationalities, Wuhan 430074, P.R. China
Gongyi Liu
Key Laboratory of Catalysis and Materials Science of Hubei Province, College of Chemistry and Materials Science, South-Central University for Nationalities, Wuhan 430074, P.R. China
Lu Lei
Key Laboratory of Catalysis and Materials Science of Hubei Province, College of Chemistry and Materials Science, South-Central University for Nationalities, Wuhan 430074, P.R. China
Aiqing Zhang
Key Laboratory of Catalysis and Materials Science of Hubei Province, College of Chemistry and Materials Science, South-Central University for Nationalities, Wuhan 430074, P.R. China

Corresponding Author(s) : Guangyong Xie

xxgyy@hotmail.com

Asian Journal of Chemistry, Vol. 26 No. 3 (2014): Vol 26 Issue 3

Abstract

A series of N-aryl-b-enaminones were efficiently prepared by acetylacetone reacted with substituted anilines in high yields without additional solvent under microwave irradiation. The most yields can reach over 80 %. Compared with traditional routes, this method needs only 15 min and simpler after-treatment procedures while owns higher yields.

Keywords

N-aryl-b-enaminones Acetylacetone Microwave Solvent-free Synthesis
Xie, G., Li, L., Liu, G., Lei, L., & Zhang, A. (2014). Solvent-Free Synthesis of N-aryl-b-Enaminones Under Microwave Irradiation. Asian Journal of Chemistry, 26(3), 937–938. https://doi.org/10.14233/ajchem.2014.15524
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