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Copyright (c) 2014 Bingqing Cao*, Qibin Huang, Molin Qing
This work is licensed under a Creative Commons Attribution 4.0 International License.
Synthesis of 25-(Thioalkyl-alkoxy)-p-tertbutylcalix[4]arene in One Reaction System
Corresponding Author(s) : Bingqing Cao*
Asian Journal of Chemistry,
Vol. 26 No. 24 (2014)
Abstract
25-(Thioalkyl-alkoxy)-p-tertbutylcalix[4]arene with self-assembled monolayers character was synthesized by two steps nucleophilic substitute reaction in NaH-THF phase with p-tertbutylcalix[4]arene and dibromodecane. The structure of product was characterized by FT-IR, 1H NMR, 13C NMR and MALDI-TOF-MS.
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References
F.F. Yang, Y.Y. Chen and S. Lin, Chin. J. Org. Chem, 22, 746 (2002).
B. Gao, Y.Q. Feng, L.S. Zhou and X. Ma, Chin. J. Org. Chem., 24, 713 (2004).
E.U. Thoden van Velzen, J.F.J. Engbersen and D.N. Reinhoudt, J. Am. Chem. Soc., 116, 3597 (1994).
K.D. Schierbaum, T. Weiss, E.U.T. van Veizen, J.F.J. Engbersen, D.N. Reinhoudt and W. Gopel, Science, 265, 1413 (1994).
B.T. Zhao, H.Y. Zhang and Y. Lui, Chin. J. Org. Chem., 25, 913 (2005).
E. Ghidini, F. Ugozzoli, R. Ungaro, S. Harkema, A. Abu El-Fadl and D.N. Reinhoudt, J. Am. Chem. Soc., 112, 6979 (1990).