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Vol. 26 No. 24 (2014)

Copyright (c) 2014 Wenfei Li1, Ruixiang Yao2, Yang Lin1, Zhanhai Yao3, Shumei Liu1

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This work is licensed under a Creative Commons Attribution 4.0 International License.

Preparation and Characterization of Reactive Type Dripping Agent Containing a-Double Bond

https://doi.org/10.14233/ajchem.2014.18377
Wenfei Li1
1College of Chemistry and Environmental Engineering, Changchun University of Science and Technology, Changchun 130022, P.R. China 2College of Chemistry, Jilin University, Changchun 130012, P.R. China 3State Key Laboratory of Polymer Physics and Chemistry, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, P.R. China *Corresponding author: E-mail: liwenfei1130@126.com
Ruixiang Yao2
1College of Chemistry and Environmental Engineering, Changchun University of Science and Technology, Changchun 130022, P.R. China 2College of Chemistry, Jilin University, Changchun 130012, P.R. China 3State Key Laboratory of Polymer Physics and Chemistry, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, P.R. China *Corresponding author: E-mail: liwenfei1130@126.com
Yang Lin1
1College of Chemistry and Environmental Engineering, Changchun University of Science and Technology, Changchun 130022, P.R. China 2College of Chemistry, Jilin University, Changchun 130012, P.R. China 3State Key Laboratory of Polymer Physics and Chemistry, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, P.R. China *Corresponding author: E-mail: liwenfei1130@126.com
Zhanhai Yao3
1College of Chemistry and Environmental Engineering, Changchun University of Science and Technology, Changchun 130022, P.R. China 2College of Chemistry, Jilin University, Changchun 130012, P.R. China 3State Key Laboratory of Polymer Physics and Chemistry, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, P.R. China *Corresponding author: E-mail: liwenfei1130@126.com
Shumei Liu1
1College of Chemistry and Environmental Engineering, Changchun University of Science and Technology, Changchun 130022, P.R. China 2College of Chemistry, Jilin University, Changchun 130012, P.R. China 3State Key Laboratory of Polymer Physics and Chemistry, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, P.R. China *Corresponding author: E-mail: liwenfei1130@126.com

Corresponding Author(s) : Wenfei Li1

Asian Journal of Chemistry, Vol. 26 No. 24 (2014)

Abstract

A reactive type dripping agent containing a double bond, sorbitan monostearate-itaconic anhydride (Span60-IAH) was synthesized with sorbitan monostearate (Span60) and itaconic anhydride as main starting materials. The chemical structures of Span60-IAH were characterized by Fourier transform infrared (FT-IR) spectroscopy and 1H NMR. The effect of reaction time on conversion of Span60-IAH was studied. The surface activity and surface tension of Span60-IAH were evaluated by a drop weight method. Thermal stability of Span60-IAH and Span60 were investigated by TGA. When residual weight (%) was 90 %, the decomposition temperature of Span60-IAH was about 28 °C higher than that of Span60. The wettability is expressed by the water contact angle.

Keywords

Dripping agent Itaconic anhydride Span60.
Li1, W., Yao2, R., Lin1, Y., Yao3, Z., & Liu1, S. (2014). Preparation and Characterization of Reactive Type Dripping Agent Containing a-Double Bond. Asian Journal of Chemistry, 26(24), 8577–8580. https://doi.org/10.14233/ajchem.2014.18377
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