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Vol. 26 No. 24 (2014)

Copyright (c) 2014 Jingyu Zhang1, Qinglong Wang2, Xuehui Hou2

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This work is licensed under a Creative Commons Attribution 4.0 International License.

Synthesis and Structure of Novel Anhydrogalactosucrose Derivative

https://doi.org/10.14233/ajchem.2014.18350
Jingyu Zhang1
1School of Pharmacy Henan University of Traditional Chinese Medicine, Zhengzhou 450008, P.R. China 2Department of Quality Detection and Management, Henan University of Animal Husbandry and Economy, Zhengzhou 450011, P.R. China *Corresponding author: Tel/Fax: +86 371 86176305; E-mail: houxh2006@163.com
Qinglong Wang2
1School of Pharmacy Henan University of Traditional Chinese Medicine, Zhengzhou 450008, P.R. China 2Department of Quality Detection and Management, Henan University of Animal Husbandry and Economy, Zhengzhou 450011, P.R. China *Corresponding author: Tel/Fax: +86 371 86176305; E-mail: houxh2006@163.com
Xuehui Hou2
1School of Pharmacy Henan University of Traditional Chinese Medicine, Zhengzhou 450008, P.R. China 2Department of Quality Detection and Management, Henan University of Animal Husbandry and Economy, Zhengzhou 450011, P.R. China *Corresponding author: Tel/Fax: +86 371 86176305; E-mail: houxh2006@163.com

Corresponding Author(s) : Jingyu Zhang1

Asian Journal of Chemistry, Vol. 26 No. 24 (2014)

Abstract

A novel anhydrogalactosucrose derivative was prepared from sucrose. Its structure was determined by single crystal X-ray diffraction analysis. The crystals are monoclinic, space group P21 with a = 5.40373(15), b = 18.3877(5), c = 7.68465(19) Å, a = 90.00, b = 103.299(3), g = 90.00°, V = 743.08(4) Å3, Z = 2, F(000) = 376.0, Dc = 1.614g/cm3, μ = 4.307 mm-1, the final R = 0.0344 and wR = 0.0881. A total of 6472 reflections were collected, of which 2732 were independent (Rint = 0.0286).

Keywords

Anhydrogalactosucrose Synthesis Crystal structure.
Zhang1, J., Wang2, Q., & Hou2, X. (2014). Synthesis and Structure of Novel Anhydrogalactosucrose Derivative. Asian Journal of Chemistry, 26(24), 8563–8565. https://doi.org/10.14233/ajchem.2014.18350
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