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Vol. 26 No. 24 (2014)

Copyright (c) 2014 Qingyun Liu*, Qingyan Jia, Hangyue Zhou, Chun Gao, Qian Shao, Guijiang Li, Bing Bian

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This work is licensed under a Creative Commons Attribution 4.0 International License.

One-Step Facile Preparation and Photoluminescence Properties of Tetrakis(4-carboxyphenyl)porphyrin Functionalized Zinc Oxide Nanostructures

https://doi.org/10.14233/ajchem.2014.16942
Qingyun Liu*
College of Chemical and Environmental Engineering, Shandong University of Science and Technology, Qingdao 266510, P.R. China *Corresponding author: Fax: +86 532 80681197; Tel: +86 532 86057757; E-mail: qyliusdu@163.com; qyliu@sdust.edu.cn
Qingyan Jia
College of Chemical and Environmental Engineering, Shandong University of Science and Technology, Qingdao 266510, P.R. China *Corresponding author: Fax: +86 532 80681197; Tel: +86 532 86057757; E-mail: qyliusdu@163.com; qyliu@sdust.edu.cn
Hangyue Zhou
College of Chemical and Environmental Engineering, Shandong University of Science and Technology, Qingdao 266510, P.R. China *Corresponding author: Fax: +86 532 80681197; Tel: +86 532 86057757; E-mail: qyliusdu@163.com; qyliu@sdust.edu.cn
Chun Gao
College of Chemical and Environmental Engineering, Shandong University of Science and Technology, Qingdao 266510, P.R. China *Corresponding author: Fax: +86 532 80681197; Tel: +86 532 86057757; E-mail: qyliusdu@163.com; qyliu@sdust.edu.cn
Qian Shao
College of Chemical and Environmental Engineering, Shandong University of Science and Technology, Qingdao 266510, P.R. China *Corresponding author: Fax: +86 532 80681197; Tel: +86 532 86057757; E-mail: qyliusdu@163.com; qyliu@sdust.edu.cn
Guijiang Li
College of Chemical and Environmental Engineering, Shandong University of Science and Technology, Qingdao 266510, P.R. China *Corresponding author: Fax: +86 532 80681197; Tel: +86 532 86057757; E-mail: qyliusdu@163.com; qyliu@sdust.edu.cn
Bing Bian
College of Chemical and Environmental Engineering, Shandong University of Science and Technology, Qingdao 266510, P.R. China *Corresponding author: Fax: +86 532 80681197; Tel: +86 532 86057757; E-mail: qyliusdu@163.com; qyliu@sdust.edu.cn

Corresponding Author(s) : Qingyun Liu*

Asian Journal of Chemistry, Vol. 26 No. 24 (2014)

Abstract

We developed facile synthetic procedure to prepare zinc oxide nanorods functionalized with a tetrakis(4-carboxyphenyl)porphyrin molecules by a better understanding of their coordination chemistry. The obtained samples are hexagonal Wurtzite structures characterized by X-ray diffraction spectra. FTIR data verify the porphyrin functionalized zinc oxide nanorods through coordination interaction between zinc of zinc oxide nanostructures and carboxylic groups of tetrakis(4-carboxyphenyl)porphyrin molecules. TEM images reveal that optimal reaction time of the uniform nanorods with sharp tips is about 60 min. A possible formation mechanism of the zinc oxide nanorods with sharp tips has also been proposed. Photoluminescence (PL) characterization of the functionalized nanorods shows that these nanorods exhibit strong emission at 460 nm, a red-shift of about 15 nm at UV wavelength (393 nm) and special optical properties in yellow-green emission, compared with that of the corresponding nanorods and nanowires in previous reports.

Keywords

Porphyrin Zinc oxide Nanorods Photoluminescence One-step.
Liu*, Q., Jia, Q., Zhou, H., Gao, C., Shao, Q., Li, G., & Bian, B. (2014). One-Step Facile Preparation and Photoluminescence Properties of Tetrakis(4-carboxyphenyl)porphyrin Functionalized Zinc Oxide Nanostructures. Asian Journal of Chemistry, 26(24), 8314–8318. https://doi.org/10.14233/ajchem.2014.16942
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