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Vol. 26 No. 20 (2014)

Copyright (c) 2014 Jamshid Khan1, Sumera Mahboob2, Mohammed A.T. Abdel-Reheem3, Riaz Ullah5, Iqbal Hussain6, Sajjad Haider7

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This work is licensed under a Creative Commons Attribution 4.0 International License.

Synthesis and Characterization of Zinc Oxide Nanoparticles by Modified Sol-Gel Method

https://doi.org/10.14233/ajchem.2014.17191
Jamshid Khan1
1School of Chemical and Material Engineering, National University of Sciences and Technology, Islamabad, Pakistan 2Center of Excellence in Science and Applied Technologies, Islamabad, Pakistan 3Research Center, College of Science, King Saud University, Riyadh, Saudi Arabia 4Biochemistry Department, Faculty of Agric. Ain Shams University, Cairo, Egypt 5Department of Chemistry Government College, Ara Khel F.R, Kohat, Pakistan 6Department of Chemistry, Islamia College, Peshawar, KPK, Pakistan 7Department of Chemical Engineering, College of Engineering, King Saud University, Riyadh, Saudi Arabia *Corresponding author: Fax: +92 51 9281314; Tel; +92 51 9060273; E-mail: afridiriaz@yahoo.com
Sumera Mahboob2
1School of Chemical and Material Engineering, National University of Sciences and Technology, Islamabad, Pakistan 2Center of Excellence in Science and Applied Technologies, Islamabad, Pakistan 3Research Center, College of Science, King Saud University, Riyadh, Saudi Arabia 4Biochemistry Department, Faculty of Agric. Ain Shams University, Cairo, Egypt 5Department of Chemistry Government College, Ara Khel F.R, Kohat, Pakistan 6Department of Chemistry, Islamia College, Peshawar, KPK, Pakistan 7Department of Chemical Engineering, College of Engineering, King Saud University, Riyadh, Saudi Arabia *Corresponding author: Fax: +92 51 9281314; Tel; +92 51 9060273; E-mail: afridiriaz@yahoo.com
Mohammed A.T. Abdel-Reheem3
1School of Chemical and Material Engineering, National University of Sciences and Technology, Islamabad, Pakistan 2Center of Excellence in Science and Applied Technologies, Islamabad, Pakistan 3Research Center, College of Science, King Saud University, Riyadh, Saudi Arabia 4Biochemistry Department, Faculty of Agric. Ain Shams University, Cairo, Egypt 5Department of Chemistry Government College, Ara Khel F.R, Kohat, Pakistan 6Department of Chemistry, Islamia College, Peshawar, KPK, Pakistan 7Department of Chemical Engineering, College of Engineering, King Saud University, Riyadh, Saudi Arabia *Corresponding author: Fax: +92 51 9281314; Tel; +92 51 9060273; E-mail: afridiriaz@yahoo.com
Riaz Ullah5
1School of Chemical and Material Engineering, National University of Sciences and Technology, Islamabad, Pakistan 2Center of Excellence in Science and Applied Technologies, Islamabad, Pakistan 3Research Center, College of Science, King Saud University, Riyadh, Saudi Arabia 4Biochemistry Department, Faculty of Agric. Ain Shams University, Cairo, Egypt 5Department of Chemistry Government College, Ara Khel F.R, Kohat, Pakistan 6Department of Chemistry, Islamia College, Peshawar, KPK, Pakistan 7Department of Chemical Engineering, College of Engineering, King Saud University, Riyadh, Saudi Arabia *Corresponding author: Fax: +92 51 9281314; Tel; +92 51 9060273; E-mail: afridiriaz@yahoo.com
Iqbal Hussain6
1School of Chemical and Material Engineering, National University of Sciences and Technology, Islamabad, Pakistan 2Center of Excellence in Science and Applied Technologies, Islamabad, Pakistan 3Research Center, College of Science, King Saud University, Riyadh, Saudi Arabia 4Biochemistry Department, Faculty of Agric. Ain Shams University, Cairo, Egypt 5Department of Chemistry Government College, Ara Khel F.R, Kohat, Pakistan 6Department of Chemistry, Islamia College, Peshawar, KPK, Pakistan 7Department of Chemical Engineering, College of Engineering, King Saud University, Riyadh, Saudi Arabia *Corresponding author: Fax: +92 51 9281314; Tel; +92 51 9060273; E-mail: afridiriaz@yahoo.com
Sajjad Haider7
1School of Chemical and Material Engineering, National University of Sciences and Technology, Islamabad, Pakistan 2Center of Excellence in Science and Applied Technologies, Islamabad, Pakistan 3Research Center, College of Science, King Saud University, Riyadh, Saudi Arabia 4Biochemistry Department, Faculty of Agric. Ain Shams University, Cairo, Egypt 5Department of Chemistry Government College, Ara Khel F.R, Kohat, Pakistan 6Department of Chemistry, Islamia College, Peshawar, KPK, Pakistan 7Department of Chemical Engineering, College of Engineering, King Saud University, Riyadh, Saudi Arabia *Corresponding author: Fax: +92 51 9281314; Tel; +92 51 9060273; E-mail: afridiriaz@yahoo.com

Corresponding Author(s) : Jamshid Khan1

Asian Journal of Chemistry, Vol. 26 No. 20 (2014)

Abstract

In the present work a modified sol-gel method is used for the synthesis of ZnO nano particles using zinc acetate dihydrate, ethylene diaminedihydrochloride and NaOH as precursors and poly(vinyl pyrrolidone) as surfactant to control the morphology and shape of synthesized ZnO nanoparticles. Poly(vinyl pyrrolidone) are used as capping agent and distilled water as solvent, using magnetic stirrer. The synthesized ZnO nano particles are dried in oven at 100 °C for 2 h and then calcinated at 500 °C in muffle furnace for 2 h. The synthesized nanoparticles were characterized by using X-ray diffraction, scanning electron microscopy, energy dispersive X-ray spectra and Fourier transform infrared spectroscopy.

Keywords

ZnO Sol-gel method Nanoparticles X-ray diffraction Scanning electron microscopy TGA FTIR.
Khan1, J., Mahboob2, S., A.T. Abdel-Reheem3, M., Ullah5, R., Hussain6, I., & Haider7, S. (2014). Synthesis and Characterization of Zinc Oxide Nanoparticles by Modified Sol-Gel Method. Asian Journal of Chemistry, 26(20), 7069–7070. https://doi.org/10.14233/ajchem.2014.17191
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