Copyright (c) 2014 AJC
This work is licensed under a Creative Commons Attribution 4.0 International License.
Synthesis and Crystal Structure of Symmetrical Organic Compound
Corresponding Author(s) : Lan-Qin Chai
Asian Journal of Chemistry,
Vol. 26 No. 16 (2014): Vol 26 Issue 16
Abstract
An unexpected symmetrical organic compound has been synthesized with higher yield under mild reaction conditions. The crystal structure of the title compound has been determined by single-crystal X-ray diffraction. It crystallizes in the trigonal space group P3221 with a = 8.679 (9) Å, b = 8.679 (9) Å, c = 17.714 (17) Å, b = 90° X, Z = 6.
Keywords
Download Citation
Endnote/Zotero/Mendeley (RIS)BibTeX
- A. Ourari, Y. Ouennoughi, D. Aggoun, M.S. Mubarak, E.M. Pasciak and D.G. Peters, Polyhedron, 67, 59 (2014).
- S. Saha, R.K. Kottalanka, P. Bhowmik, S. Jana, K. Harms, T.K. Panda, S. Chattopadhyay and H.P. Nayek, J. Mol. Struct., 1061, 26 (2014).
- R.N. Patel, A. Singh, V.P. Sondhiya, Y. Singh, K.K. Shukla, D.K. Patel and R. Pandey, J. Coord. Chem., 65, 795 (2012).
- M. Kalanithi, M. Rajarajan and P. Tharmaraj, J. Coord. Chem., 64, 842 (2011).
- C.J. Dhanaraj, J. Johnson, J. Joseph and R.S. Joseyphus, J. Coord. Chem., 66, 1416 (2013).
- W.K. Dong, Y.X. Sun, Y.P. Zhang, L. Li, X.N. He and X.L. Tang, Inorg. Chim. Acta, 362, 117 (2009).
- H.Y. Han, Y.L. Song, H.W. Hou, Y.T. Fan and Y. Zhu, J. Chem. Soc., Dalton Trans., 1972 (2006).
- M.E. Braun, C.D. Steffek, J. Kim, P.G. Rasmussen and O.M. Yaghi, Chem. Commun., 24, 2532 (2001).
- N.L. Rosi, M. Eddaoudi, J. Kim, M. O'Keeffe and O.M. Yaghi, CrystEngComm., 4, 401 (2002).
- M. Eddaoudi, D.B. Moler, H. Li, B. Chen, T.M. Reineke, M. O'Keeffe and O.M. Yaghi, Acc. Chem. Res., 34, 319 (2001).
- L.Q. Chai, G. Liu, Y.L. Zhang, J.J. Huang and J.F. Tong, J. Coord. Chem., 66, 3926 (2013).
- Bruker, SAINT and SMART, Bruker AXS Inc., Madison,WI, USA (2001).
- G.M. Sheldrick, SHELXS97, Program for Crystal Structure Determination, University of Göttingen, Germany (1996).
- G.M. Sheldrick, SADABS, University of Göttingen, Göttingen, Germany (2001).
- G.M. Sheldrick, Acta Crystallogr. A, 64, 112 (2008)
References
A. Ourari, Y. Ouennoughi, D. Aggoun, M.S. Mubarak, E.M. Pasciak and D.G. Peters, Polyhedron, 67, 59 (2014).
S. Saha, R.K. Kottalanka, P. Bhowmik, S. Jana, K. Harms, T.K. Panda, S. Chattopadhyay and H.P. Nayek, J. Mol. Struct., 1061, 26 (2014).
R.N. Patel, A. Singh, V.P. Sondhiya, Y. Singh, K.K. Shukla, D.K. Patel and R. Pandey, J. Coord. Chem., 65, 795 (2012).
M. Kalanithi, M. Rajarajan and P. Tharmaraj, J. Coord. Chem., 64, 842 (2011).
C.J. Dhanaraj, J. Johnson, J. Joseph and R.S. Joseyphus, J. Coord. Chem., 66, 1416 (2013).
W.K. Dong, Y.X. Sun, Y.P. Zhang, L. Li, X.N. He and X.L. Tang, Inorg. Chim. Acta, 362, 117 (2009).
H.Y. Han, Y.L. Song, H.W. Hou, Y.T. Fan and Y. Zhu, J. Chem. Soc., Dalton Trans., 1972 (2006).
M.E. Braun, C.D. Steffek, J. Kim, P.G. Rasmussen and O.M. Yaghi, Chem. Commun., 24, 2532 (2001).
N.L. Rosi, M. Eddaoudi, J. Kim, M. O'Keeffe and O.M. Yaghi, CrystEngComm., 4, 401 (2002).
M. Eddaoudi, D.B. Moler, H. Li, B. Chen, T.M. Reineke, M. O'Keeffe and O.M. Yaghi, Acc. Chem. Res., 34, 319 (2001).
L.Q. Chai, G. Liu, Y.L. Zhang, J.J. Huang and J.F. Tong, J. Coord. Chem., 66, 3926 (2013).
Bruker, SAINT and SMART, Bruker AXS Inc., Madison,WI, USA (2001).
G.M. Sheldrick, SHELXS97, Program for Crystal Structure Determination, University of Göttingen, Germany (1996).
G.M. Sheldrick, SADABS, University of Göttingen, Göttingen, Germany (2001).
G.M. Sheldrick, Acta Crystallogr. A, 64, 112 (2008)