Copyright (c) 2021 AJC
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Preparation, Characterization and Applications of Chitosan-Nanosilica-Graphene Oxide Nanocomposite
Corresponding Author(s) : A. Sahila Grace
Asian Journal of Chemistry,
Vol. 33 No. 11 (2021): Vol 33 Issue 11, 2021
Abstract
In present study, a simple low cost method was used to prepare chitosan-nanosilica-graphene oxide (CS-NSi-GO) nanocomposite. Nanosilica and graphene oxide were synthesized from coconut husk ash and chitosan was synthesized from shrimp shell. Nanosilica was synthesized from coconut husk ash with alkaline extraction using sodium hydroxide followed by precipitation method using sulphuric acid. Graphene oxide was synthesized from the oxidative treatment of the raw material of coconut husk ash. After the synthesis of silica, the carbonized graphite was collected and treated by modified Hummer’s method. The CS-NSi-GO nanocomposite was prepared by condense polymerization method. Various analytical methods such as Fourier transform infrared (FTIR) spectroscopy, Fourier transform Raman (FT-Raman) spectroscopy, scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDAX) and transmission electron microscopy (TEM) were used to characterize the CS-NSi-GO nanocomposite. Eventually antibacterial, antifungal, antioxidant and cytotoxicity of the prepared nanocomposite were also evaluated.
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- S. Khoee, R. Bafkary and F. Fayyazi, J. Sol-Gel Sci. Technol., 81, 493 (2017); https://doi.org/10.1007/s10971-016-4213-y
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References
S. Khoee, R. Bafkary and F. Fayyazi, J. Sol-Gel Sci. Technol., 81, 493 (2017); https://doi.org/10.1007/s10971-016-4213-y
N. Morin-Crini, E. Lichtfouse, G. Torri and G. Crini, Environ. Chem. Lett., 17, 1667 (2019); https://doi.org/10.1007/s10311-019-00904-x
A. Suri, V. Khandegar and P.J. Kaur, Groundw. Sustain. Dev., 12, 100515 (2021); https://doi.org/10.1016/j.gsd.2020.100515
J. Diosa, F. Guzman, C. Bernal and M. Mesa, J. Mater. Res. Technol., 9, 890 (2020); https://doi.org/10.1016/j.jmrt.2019.11.029
R.R. Castillo, D. Lozano and M. Vallet-Regí, Pharmaceutics, 12, 432 (2020); https://doi.org/10.3390/pharmaceutics12050432
T.M. M. Ways, K.W. Ng, W.M. Lau and V.V. Khutoryanskiy, Pharmaceutics, 12, 751 (2020); https://doi.org/10.3390/pharmaceutics12080751
C. Rejeeth, T.C. Nag and S. Kannan, Cancer Nanotechnol., 4, 127 (2013); https://doi.org/10.1007/s12645-013-0043-6
S.A. Qamar, M. Ashiq, M. Jahangeer, A. Riasat and M. Bilal, Case Stud. Chem. Environ. Eng., 2, 100021 (2020); https://doi.org/10.1016/j.cscee.2020.100021
T.M. Budnyak, I.V. Pylypchuk, V.A. Tertykh, E.S. Yanovska and D. Kolodynska, Nanoscale Res. Lett., 10, 87 (2015); https://doi.org/10.1186/s11671-014-0722-1
Q. Xu, T. Ji, S.J. Gao, Z. Yang and N. Wu, Materials, 12, 39 (2018); https://doi.org/10.3390/ma12010039
S.K. Tiwari, S. Sahoo, N. Wang and A. Huczko, J. Sci.-Adv. Mater. Dev., 5, 10 (2020); https://doi.org/10.1016/j.jsamd.2020.01.006
K. Narasimharao, G. Venkata Ramana, D. Sreedhar and V. Vasudevarao, J. Mar. Sci. Eng., 5, 284 (2016); https://doi.org/10.4172/2169-0022.1000284
G. Speranza, J. Carbon Res., 5, 84 (2019); https://doi.org/10.3390/c5040084
M. Sabzevari, D.E. Cree and L.D. Wilson, ACS Omega, 3, 13045 (2018); https://doi.org/10.1021/acsomega.8b01871
P.P. Zuo, H.F. Feng, Z.Z. Xu, L.F. Zhang, Y.L. Zhang, W. Xia and W.Q. Zhang, Chem. Cent. J., 7, 39 (2013); https://doi.org/10.1186/1752-153X-7-39
D. Yuan, C.M. Ellis and J.J. Davis, Materials, 13, 3795 (2020); https://doi.org/10.3390/ma13173795
Y. Du, L. Huang, Y. Wang, K. Yang, Z. Zhang, Y. Wang, M.J. Kipper, L.A. Belfiore and J. Tang, J. Mater. Sci., 55, 11188 (2020); https://doi.org/10.1007/s10853-020-04774-5
C. Brasselet, G. Pierre, P. Dubessay, M. Dols-Lafargue, J. Coulon, J. Maupeu, A. Vallet-Courbin, H. de Baynast, T. Doco, P. Michaud and C. Delattre, Appl. Sci., 9, 1321 (2019); https://doi.org/10.3390/app9071321
W.K. Alderton, C.E. Cooper and R.G. Knowels, J. Biol. Chem., 357, 593 (2001); https://doi.org/10.1042/0264-6021:3570593