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Synthesis and Structural Characterization of Copper(II) Complex with Asymmetrical Salen-Type Bisoxime Ligand
Corresponding Author(s) : Wen-You Li
Asian Journal of Chemistry,
Vol. 25 No. 9 (2013): Vol 25 Issue 9
Abstract
A new mononuclear Cu(II) complex, [CuL], has been synthesized by the reaction of copper(II) acetate tetrahydrate with H2L (H2L = 4-bromo-6'-methoxy-2,2'-[ethylenediyldioxybis(nitrilomethylidyne)]diphenol). X-Ray crystallographic analysis reveals that the complex crystallizes in the monoclinic system, space group P2(1) and the unit cell contains two crystallographically independent but chemically identical molecules which interlink each other into a 1D infinite chain through four strong intermolecular O12-H12C···O4, O12-H12D···O5, O11-H11C···O9 and O11-H11D···O10 hydrogen bonds.
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- W.K. Dong, J.G. Duan, Y.H. Guan, J.Y. Shi and C.Y. Zhao, Inorg. Chim. Acta, 362, 1129 (2009).
- W.K. Dong, X.N. He, H.B. Yan, Z.W. Lv, X. Chen, C.Y. Zhao and X.L. Tang, Polyhedron, 28, 1419 (2009).
- M.A. Subhan, T. Suzuki and S. Kaizaki, J. Chem. Soc., 1416 (2002).
- W.K. Dong, Y.X. Sun, Y.P. Zhang, L. Li, X.N. He and X.L. Tang, Inorg. Chim. Acta, 362, 117 (2009).
- W.K. Dong, Y.X. Sun, S.J. Xing, Y. Wang and X.H. Gao, Z. Naturforsch., 67b, 197 (2012).
- A. Bencini, C. Benelli,A. Caneschi, R.L. Carlin,A. Dei and D. Gatteschi, J. Am. Chem. Soc., 107, 8128 (1985).
- W.K. Dong and J.G. Duan, J. Coord. Chem., 61, 781 (2007).
- M. Sasaki, K. Manseki, H. Horiuchi, M. Kumagai and H. Okawa, J. Chem. Soc., 259 (2000).
- I. Sasaki, D. Pujol and A. Gaudemer, Inorg. Chim. Acta, 134, 53 (1987).
- W.K. Dong, J.F. Tong, Y.X. Sun, S.S. Gong and L. Li, Synth. React. Inorg. Met.-Org. Nano-Met. Chem., 41, 155 (2011).
- H.L. Wu, X.C. Huang, J.K. Yuan, F. Kou, F. Jia, B. Liu and Y. Bai, Z. Naturforsch., 66b, 1049 (2011).
- W.K. Dong, G. Wang, S.S. Gong, J.F. Tong, Y.X. Sun and X.H. Gao, Transition Met. Chem., 37, 271 (2012).
- W.K. Dong, X.N. He, C.M. Dong, L. Wang, J.K. Zhong, X. Chen and T.Z. Yu, Z. Kristallogr. New Cryst. Struct., 222, 289 (2007).
References
W.K. Dong, J.G. Duan, Y.H. Guan, J.Y. Shi and C.Y. Zhao, Inorg. Chim. Acta, 362, 1129 (2009).
W.K. Dong, X.N. He, H.B. Yan, Z.W. Lv, X. Chen, C.Y. Zhao and X.L. Tang, Polyhedron, 28, 1419 (2009).
M.A. Subhan, T. Suzuki and S. Kaizaki, J. Chem. Soc., 1416 (2002).
W.K. Dong, Y.X. Sun, Y.P. Zhang, L. Li, X.N. He and X.L. Tang, Inorg. Chim. Acta, 362, 117 (2009).
W.K. Dong, Y.X. Sun, S.J. Xing, Y. Wang and X.H. Gao, Z. Naturforsch., 67b, 197 (2012).
A. Bencini, C. Benelli,A. Caneschi, R.L. Carlin,A. Dei and D. Gatteschi, J. Am. Chem. Soc., 107, 8128 (1985).
W.K. Dong and J.G. Duan, J. Coord. Chem., 61, 781 (2007).
M. Sasaki, K. Manseki, H. Horiuchi, M. Kumagai and H. Okawa, J. Chem. Soc., 259 (2000).
I. Sasaki, D. Pujol and A. Gaudemer, Inorg. Chim. Acta, 134, 53 (1987).
W.K. Dong, J.F. Tong, Y.X. Sun, S.S. Gong and L. Li, Synth. React. Inorg. Met.-Org. Nano-Met. Chem., 41, 155 (2011).
H.L. Wu, X.C. Huang, J.K. Yuan, F. Kou, F. Jia, B. Liu and Y. Bai, Z. Naturforsch., 66b, 1049 (2011).
W.K. Dong, G. Wang, S.S. Gong, J.F. Tong, Y.X. Sun and X.H. Gao, Transition Met. Chem., 37, 271 (2012).
W.K. Dong, X.N. He, C.M. Dong, L. Wang, J.K. Zhong, X. Chen and T.Z. Yu, Z. Kristallogr. New Cryst. Struct., 222, 289 (2007).