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Synthesis and Crystal Structure of 2,2'-(1,2-Ethylenedioxy)bisbenzaldehyde O,O'-Diethyldioxime
Corresponding Author(s) : Li Zhao
Asian Journal of Chemistry,
Vol. 25 No. 9 (2013): Vol 25 Issue 9
Abstract
The compound, 2,2'-(1,2-ethylenedioxy)-bis-benzaldehyde O,O'-diethyldioxime, has been synthesized by 2,2'-(1,2-ethylenedioxy)-bis-benzaldehyde O,O'-diethyldioxime and ethoxyamine hydrochloride in ethanolic solution and characterized structurally by X-ray crystallography. The molecule of the title compound adopts an extended conformation where the two oxime groups are apart from each other. The two benzene rings are parallel to each other. In the crystal structure, intermolecular C7-H7···O2 hydrogen bonds link the molecules forming an infinite 1D chain-like supramolecular structure.
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- W.K. Dong, Y.X. Sun, S.J. Xing, Y. Wang and X.H. Gao, Z. Naturforsch., 67b, 197 (2012).
- W.K. Dong, J.F. Tong, Y.X. Sun, S.S. Gong and L. Li, Synth. React. Inorg. Met.-Org. Nano-Met. Chem., 41, 155 (2011).
- W.K. Dong, G. Wang, S.S. Gong, J.F. Tong, Y.X. Sun and X.H. Gao, Transition Met. Chem., 37, 271 (2012).
- W.K. Dong, Y.X. Sun, Y.P. Zhang, L. Li, X.N. He and X.L. Tang, Inorg. Chim. Acta, 362, 117 (2009).
- W.K. Dong, X.N. He, H.B. Yan, Z.W. Lv, X. Chen, C.Y. Zhao and X.L. Tang, Polyhedron, 28, 1419 (2009).
- J.P. Costes, F. Dahan and A. Dupuis, Inorg. Chem., 39, 165 (2000).
- S.S. Sun, C.L. Stern, S.T. Nguyen and J.T. Hupp, J. Am. Chem. Soc., 126, 6314 (2004).
- A.K. Sharma, F. Lloret and R. Mukherjee, Inorg. Chem., 46, 5128 (2007).
- C. Policar, F. Lambert, M. Cesario and I. Morgenstern-badarau, Eur. J. Inorg. Chem., 12, 2201 (1999).
- D.A. Atwood and M.J. Harvey, Chem. Rev., 101, 37 (2001).
- I.M. Atkinson, L.F. Lindoy, O.A. Matthews, G.V. Meehan,A.N. Sobolev and A.H. White, Aust. J. Chem., 47, 1155 (1994).
- W.K. Dong, J. Yao, Y.X. Sun, L. Li and J.C. Wu, Synth. React. Inorg. Met.-Org. Nano-Met. Chem., 40, 521 (2010).
- G.M. Sheldrick, Acta Crystallogr., A64, 112 (2008).
- W.K. Dong, Y.X. Sun, G.H. Liu, L. Li, X.Y. Dong and X.H. Gao, Z. Anorg. Allg. Chem., 638, 1370 (2012).
- W.K. Dong, J.G. Duan, Y.H. Guan, J.Y. Shi and C.Y. Zhao, Inorg. Chim. Acta, 362, 1129 (2009).
- H.L. Wu, X.C. Huang, J.K. Yuan, F. Kou, F. Jia, B. Liu and Y. Bai, Z. Naturforsch., 66b, 1049 (2011).
References
W.K. Dong, Y.X. Sun, S.J. Xing, Y. Wang and X.H. Gao, Z. Naturforsch., 67b, 197 (2012).
W.K. Dong, J.F. Tong, Y.X. Sun, S.S. Gong and L. Li, Synth. React. Inorg. Met.-Org. Nano-Met. Chem., 41, 155 (2011).
W.K. Dong, G. Wang, S.S. Gong, J.F. Tong, Y.X. Sun and X.H. Gao, Transition Met. Chem., 37, 271 (2012).
W.K. Dong, Y.X. Sun, Y.P. Zhang, L. Li, X.N. He and X.L. Tang, Inorg. Chim. Acta, 362, 117 (2009).
W.K. Dong, X.N. He, H.B. Yan, Z.W. Lv, X. Chen, C.Y. Zhao and X.L. Tang, Polyhedron, 28, 1419 (2009).
J.P. Costes, F. Dahan and A. Dupuis, Inorg. Chem., 39, 165 (2000).
S.S. Sun, C.L. Stern, S.T. Nguyen and J.T. Hupp, J. Am. Chem. Soc., 126, 6314 (2004).
A.K. Sharma, F. Lloret and R. Mukherjee, Inorg. Chem., 46, 5128 (2007).
C. Policar, F. Lambert, M. Cesario and I. Morgenstern-badarau, Eur. J. Inorg. Chem., 12, 2201 (1999).
D.A. Atwood and M.J. Harvey, Chem. Rev., 101, 37 (2001).
I.M. Atkinson, L.F. Lindoy, O.A. Matthews, G.V. Meehan,A.N. Sobolev and A.H. White, Aust. J. Chem., 47, 1155 (1994).
W.K. Dong, J. Yao, Y.X. Sun, L. Li and J.C. Wu, Synth. React. Inorg. Met.-Org. Nano-Met. Chem., 40, 521 (2010).
G.M. Sheldrick, Acta Crystallogr., A64, 112 (2008).
W.K. Dong, Y.X. Sun, G.H. Liu, L. Li, X.Y. Dong and X.H. Gao, Z. Anorg. Allg. Chem., 638, 1370 (2012).
W.K. Dong, J.G. Duan, Y.H. Guan, J.Y. Shi and C.Y. Zhao, Inorg. Chim. Acta, 362, 1129 (2009).
H.L. Wu, X.C. Huang, J.K. Yuan, F. Kou, F. Jia, B. Liu and Y. Bai, Z. Naturforsch., 66b, 1049 (2011).