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Synthesis and Supramolecular Structure of 5,5'-Dihydroxy-2,2'-[1,1'-(propane-1,3-diyldioxydinitrilo)dimethylidyne]diphenol
Corresponding Author(s) : Wen-Kui Dong
Asian Journal of Chemistry,
Vol. 25 No. 8 (2013): Vol 25 Issue 8
Abstract
The compound, 5,5'-dihydroxy-2,2'-[1,1'-(propane-1,3-diyldioxydinitrilo)dimethylidyne]diphenol with the molecular formula C17H18N2O6, assumes a cis conguration in which two phenoloxime moieties adopts an extended form. The dihedral angle between the two benzene rings of the molecule is 1.83(3)º. There are two fairly strong intramolecular O3-H3···N1 and O5-H5···N2 hydrogen bonds. Each compound molecule links three other neighboring molecules through two pairs of intermolecular O6-H6···O3 and O4-H4···O6 hydrogen-bonding interactions into an infinite wave-like 2D-layer supramolecular structure parallel to the ab crystallographic plane.
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- S. Akine, W.K. Dong and T. Nabeshima, Inorg. Chem., 45, 4677 (2006).
- S. Akine, T. Taniguchi and T. Nabeshima, Angew. Chem., Int. Ed., 41, 4670 (2002).
- J. Tisato, F. Refosco and F. Bandoli, Coord. Chem. Rev., 135-136, 325 (1994).
- E.C. Niederhoffer, J.H. Timmons and A.E. Martell, Chem. Rev., 84, 137 (1984).
- S.S. Sundari,A. Dhathathreyan, M. Kanthimathi and U.N. Balachandran, Langmuir, 13, 4923 (1997).
- P.G. Lacroix, Eur. J. Inorg. Chem., 2, 339 (2001).
- W.K. Dong, G. Wang, S.S. Gong, J.F. Tong, Y.X. Sun and X.H. Gao, Transition Met. Chem., 37, 271 (2012).
- W.K. Dong, X.N. He, H.B. Yan, Z.W. Lv, X. Chen, C.Y. Zhao and X.L. Tang, Polyhedron, 28, 1419 (2009).
- J.G. Duan, C.M. Dong, J.Y. Shi, L. Wu and W.K. Dong, Acta Cryst., E63, o2704 (2007).
- W.K. Dong and J.H. Feng, Acta Cryst., E62, o3577 (2006).
- W.K. Dong, J.H. Feng and X.Q. Yang, Z. Kristallogr. New Cryst. Struct., 221, 447 (2006).
- W.K. Dong, J.Y. Shi, Y.X. Sun, L. Wang, J.G. Duan, J.K. Zhong and L. Xu, Analyst Sci., 23, x167 (2007).
- H.L. Wu, X.C. Huang, J.K. Yuan, F. Kou, F. Jia, B. Liu and Y. Bai, Z. Naturforsch., 66b, 1049 (2011).
- W.K. Dong, Y.X. Sun, Y.P. Zhang, L. Li, X.N. He and X.L. Tang, Inorg. Chim. Acta, 362, 117 (2009).
- W.K. Dong, J.G. Duan, Y.H. Guan, J.Y. Shi and C.Y. Zhao, Inorg. Chim. Acta, 362, 1129 (2009).
- H.L. Wu, K.T. Wang, F. Kou, F. Jia, B. Liu, J.K. Yuan and Y. Bai, J. Coord. Chem. 64, 2676 (2010).
References
S. Akine, W.K. Dong and T. Nabeshima, Inorg. Chem., 45, 4677 (2006).
S. Akine, T. Taniguchi and T. Nabeshima, Angew. Chem., Int. Ed., 41, 4670 (2002).
J. Tisato, F. Refosco and F. Bandoli, Coord. Chem. Rev., 135-136, 325 (1994).
E.C. Niederhoffer, J.H. Timmons and A.E. Martell, Chem. Rev., 84, 137 (1984).
S.S. Sundari,A. Dhathathreyan, M. Kanthimathi and U.N. Balachandran, Langmuir, 13, 4923 (1997).
P.G. Lacroix, Eur. J. Inorg. Chem., 2, 339 (2001).
W.K. Dong, G. Wang, S.S. Gong, J.F. Tong, Y.X. Sun and X.H. Gao, Transition Met. Chem., 37, 271 (2012).
W.K. Dong, X.N. He, H.B. Yan, Z.W. Lv, X. Chen, C.Y. Zhao and X.L. Tang, Polyhedron, 28, 1419 (2009).
J.G. Duan, C.M. Dong, J.Y. Shi, L. Wu and W.K. Dong, Acta Cryst., E63, o2704 (2007).
W.K. Dong and J.H. Feng, Acta Cryst., E62, o3577 (2006).
W.K. Dong, J.H. Feng and X.Q. Yang, Z. Kristallogr. New Cryst. Struct., 221, 447 (2006).
W.K. Dong, J.Y. Shi, Y.X. Sun, L. Wang, J.G. Duan, J.K. Zhong and L. Xu, Analyst Sci., 23, x167 (2007).
H.L. Wu, X.C. Huang, J.K. Yuan, F. Kou, F. Jia, B. Liu and Y. Bai, Z. Naturforsch., 66b, 1049 (2011).
W.K. Dong, Y.X. Sun, Y.P. Zhang, L. Li, X.N. He and X.L. Tang, Inorg. Chim. Acta, 362, 117 (2009).
W.K. Dong, J.G. Duan, Y.H. Guan, J.Y. Shi and C.Y. Zhao, Inorg. Chim. Acta, 362, 1129 (2009).
H.L. Wu, K.T. Wang, F. Kou, F. Jia, B. Liu, J.K. Yuan and Y. Bai, J. Coord. Chem. 64, 2676 (2010).