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Efficient Synthesis of 1,3-Adamantanedicarboxylic Acid and 1,3-Diaminoadamantane
Corresponding Author(s) : Hua Zhu
Asian Journal of Chemistry,
Vol. 25 No. 7 (2013): Vol 25 Issue 7
Abstract
1,3-Adamantane dicarboxylic acid was efficiently synthesized from 1-adamantane carboxylic acid by one-pot method. 1,3-Diaminoadamantane was synthesized from 1,3-adamantane dicarboxylic acid via amidation reaction and Hofmann degradation. The structure was confirmed by NMR spectra, etc.
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References
R.A. Bright, D.K. Shay, B. ShuN.J. Cox and A.I. Klimov, J. Am. Med. Assoc., 295, 891 (2006).
V.M. Deyde, X.Y. Xu, R.A. Bright, M. Shaw, C.B. Smith, Y. Zhang, Y. Shu, L.V. Gubareva, N.J. Cox and A.I. Klimov, J. Infect. Dis., 196, 249 (2007).
K. Pabbaraju, K.C.Y. Ho, S. Wong, S. Shokoples, X.L. Pang, K. Fonseca and J.D. Fox, Antiviral Res., 79, 81 (2008).
A.S. Mathews, I. Kim and C.S. Ha, J. Appl. Polym. Sci., 102, 3316 (2006).
A.S. Mathews, I. Kim and C.S. Ha, J. Polym. Sci.: Part A: Polym. Chem., 44, 5254 (2006).
Y.-T. Chern and W.-H. Chung, J. Polym. Sci. Part A: Polym. Chem., 34, 117 (1996).
H. Seino, A. Mochizuki and M. Ueda, J. Polym. Sci. Part A: Polym. Chem., 37, 3584 (1999).
A.P. Khardin, S.S. Radchenko and S.S. Novikov, Russ. Chem. Bull., 21, 2036 (1972).
E.V. Vashkevich, N.Y. Yurashevich, N.G. Kozlov, V. I. Potkin and T.N. Potkina, Russ. J. Appl. Chem., 74, 1892 (2001).
J.C. Jin, Y.N. Zhang, Y.Y. Wang, J.-Q. Liu, Z. Dong and Q.-Z. Shi, Chem.-An Asian J., 5, 1611 (2010).
D.Matsukawa, H. Wakayama, K. Mitsukura, H. Okamura, Y. Hirai and M. Shirai, J. Mater. Chem., 19, 4085 (2009).