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Microwave-Assisted Solvothermal Synthesis and Characterization of M3V2O8 (M = Ca, Cd) Nanoparticles
Corresponding Author(s) : Chang Sung Lim
Asian Journal of Chemistry,
Vol. 25 No. 6 (2013): Vol 25 Issue 6
Abstract
M3V2O8 (M = Ca, Cd) nanoparticles were synthesized successfully using a facile microwave solvothermal route followed by further heat-treatment. Well-crystallized Ca3V2O8 and Cd3V2O8 nanoparticles were formed after heat-treatment at 600 ºC for 3 h showing a fine and homogeneous morphology with particle sizes of 50-150 nm for Ca3V2O8 and 50-200 nm for Cd3V2O8. The synthesized Ca3V2O8 and Cd3V2O8 nanoparticles were characterized by X-ray diffraction, Fourier transform infrared spectroscopy and transmission electron microscopy. The optical properties were investigated by photoluminescence emission and Raman spectroscopy.
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References
T. Nakajima, M. Isobe, T. Tsuchiya, Y. Ueda and T. Kumagai, J. Luminescence, 129, 1598 (2009).
F. Yen, R.P. Chaudhury, E. Galstyan, B. Lorenz, Y.Q. Wang, Y.Y. Sun and C.W. Chu, Physica B, 403, 1487 (2008).
N. Rogado, G. Lawes, D.A. Huse, A.P. Ramirez and R.J. Cava, Solid State Commun., 124, 229 (2002).
D. Wang, Z. Zou and J. Ye, Res. Chem. Intermed., 31, 433 (2005).
M. Kurzawa and A. Blonska-Tabero, J. Therm. Anal. Calorim., 77, 17 (2004).
P. Parhi and V. Manivannan, Mat. Res. Bull., 43, 2966 (2008).
S.S. Kim, H. Ikuta and M. Wakihara, Solid State Ionics, 139, 57 (2001).
P. Parhi, V. Manivannan, S. Kohli and P. Mccurdy, Bull. Mater. Sci., 31, 885 (2008).
V. Manivannan, P. Parhi and J. Howard, J. Cryst. Growth, 310, 2793 (2008).
R. Szymczak, M. Baran, J. Fink-Finowicki, B. Krzymanska, P. Aleshkevych, H. Szymczak, S.N. Barilo, G.L. Bychkov and S.V. Shiryaev, J. Non-Crystalline Solids, 354, 4186 (2008).
S. Das, A.K. Mukhopadhyay, S. Datta and D. Basu, Bull. Mater. Sci., 32, 1 (2009).
K.P.F. Siqueira, R.L. Moreira, M. Valadares and A. Dias, J. Mater. Sci., 45, 6083 (2010).
J.C. Sczancoski, L.S. Cavalcante, M.R. Joya, J.A. Varela, P.S. Pizani and E. Longo, Chem. Eng. J., 140, 632 (2008).
J. Bi, L. Wu, Z. Li, Z. Ding, X. Wang and X. Fu, J. Alloys Comp., 480, 684 (2009).
T. Thongtem, A. Phuruangrant and S. Thongtom, Curr. Appl. Phys., 8, 189 (2008).
Y. Toyozawa and M. Inoue, J. Phys. Soc. Jpn., 21, 1663 (1966).
E.G. Reut, Izv. Akad. Nauk SSSR, Ser. Fiz., 43, 1186 (1979).
Y. Zhang, N.A.W. Holzwarth and R.T. Williams, Phys. Rev. B, 57, 12738 (1998).
J. Van Tol and J.H. Van Der Waals, Mol. Phys., 88, 803 (1996).
V.B. Mikhailik, H. Kraus, D. Wahl and M.S. Mykhaylyk, Phys. Status Solid B, 242, R17 (2005).
T.T. Basiev, A.A. Sobol, P.G. Zverev, L.I. Ivleva, V.V. Osiko and R.C. Powell, Opt. Mater., 11, 307 (1999).