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Determination of Arsenic in Panax notoginseng by Hydride Generation Atomic Fluorescence Spectrometry
Corresponding Author(s) : Wei Liu
Asian Journal of Chemistry,
Vol. 25 No. 6 (2013): Vol 25 Issue 6
Abstract
To determine the total arsenic in Panax notoginseng a hydride generation atomic fluorescence spectrometry method was developed by atomic fluorescence spectrometry (AFS-3100). The samples were pretreated by high pressure digest. The experimental conditions were studied and optimized. There was a good linear relationship between the fluorescence intensity and arsenic concentration in the range of 0-80 μg L-1 with a correlation coefficient of 0.9995, while the detection limit was 0.036 μg L-1, a relative standard deviation of 1.7 % arsenic in the samples was 0.391 μg g-1 and a recovery range of 90.7-103.5 % was obtained.
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- E.S.J. Harris, S.G. Cao, B.A. Littlefield, J.A. Craycroft, R. Scholten, T. Kaptchuk, Y.L. Fu, W.Q. Wang, Y. Liu, H.B. Chen, Z.Z. Zhao, J. Clardy, A.D. Woolf and D.M. Eisenberg, Sci. Total Environ., 409, 4297 (2011).
- S.Q. Chen and B. Chen, Procedia Environ. Sci., 5, 153 (2011).
- U. Injang, P. Noyrod, W. Siangproh, W. Dungchai, S. Motomizu and O. Chailapakul, Anal. Chim. Acta, 668, 54 (2010).
- A. Moutsatsou, E. Chalarakis and G. Zarangas, J. Hazard. Mater., 96, 53 (2003).
- GB 2762-2005, The Tolerance Limit of Arsenic in Food.
References
E.S.J. Harris, S.G. Cao, B.A. Littlefield, J.A. Craycroft, R. Scholten, T. Kaptchuk, Y.L. Fu, W.Q. Wang, Y. Liu, H.B. Chen, Z.Z. Zhao, J. Clardy, A.D. Woolf and D.M. Eisenberg, Sci. Total Environ., 409, 4297 (2011).
S.Q. Chen and B. Chen, Procedia Environ. Sci., 5, 153 (2011).
U. Injang, P. Noyrod, W. Siangproh, W. Dungchai, S. Motomizu and O. Chailapakul, Anal. Chim. Acta, 668, 54 (2010).
A. Moutsatsou, E. Chalarakis and G. Zarangas, J. Hazard. Mater., 96, 53 (2003).
GB 2762-2005, The Tolerance Limit of Arsenic in Food.