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An Intriguing Multinuclear Cluster Based on Zinc and Benzotriazole Under Solvothermal Synthesis
Corresponding Author(s) : Si-Cai Xie
Asian Journal of Chemistry,
Vol. 25 No. 6 (2013): Vol 25 Issue 6
Abstract
The intriguing multinuclear cluster [compound 1, Zn9(btz)12(CH3COO)6, btz = benzotriazole] was obtained by solvothermal reactions using zinc(II) nitrate and benzotriazole and its crystal structure was solved from conventional single-crystal X-ray data. Crystal data for compound Zn9(btz)12(CH3COO)6: triclinic space group P-1, a = 13.0714(4) Å, b = 14.0576(4) Å, c = 16.0683(5) Å, a = 69.265(3)º, b = 78.194(2)º, g = 65.436(3)º, V = 2505.71(13) Å3 and Z = 1.
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- J.G. Haasnoot, Coord. Chem. Rev., 131, 200 (2000).
- X.L. Wang, C. Qin, E.B. Wang, Z.M. Su, L. Xu and S.R. Batten, Chem. Commun., 4789 (2005).
- X.L. Wang, C. Qin, E.B. Wang, Z.-M. Su, Y.G. Li and L. Xu, Angew. Chem., Int. Ed., 45, 7411 (2006).
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- Z.Q. Jiang, Asian J. Chem., 25, 2353 (2013).
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- G.M. Sheldrick, SHELXTL97, Program for the Refinement of Crystal Structure, University of Gottingen, Germany (1997).
References
J.G. Haasnoot, Coord. Chem. Rev., 131, 200 (2000).
X.L. Wang, C. Qin, E.B. Wang, Z.M. Su, L. Xu and S.R. Batten, Chem. Commun., 4789 (2005).
X.L. Wang, C. Qin, E.B. Wang, Z.-M. Su, Y.G. Li and L. Xu, Angew. Chem., Int. Ed., 45, 7411 (2006).
X.L. Wang, C. Qin, E.B. Wang and Z.M. Su, Chem.-Eur. J., 12, 2680 (2006).
Z.Q. Jiang, Asian J. Chem., 25, 2353 (2013).
X.L. Wang, C. Qin, Y.Q. Lan, K.Z. Shao, Z.M. Su and E.B. Wang, Chem. Commun., 410 (2009).
G.M. Sheldrick, SHELXTL97, Program for the Refinement of Crystal Structure, University of Gottingen, Germany (1997).