Production of TiO2 Nano-Rods Using Combination of Sol-Gel and Electrophoretic Methods

Hassan Nosrati; Mehran Shafi Hosseini; Mohammad Nemati; Ahmad Samariha

doi:10.14233/ajchem.2013.14250

Issue

Vol. 25 No. 6 (2013): Vol 25 Issue 6

Issue Published : December 26, 2012

This work is licensed under a Creative Commons Attribution 4.0 International License.

Production of TiO2 Nano-Rods Using Combination of Sol-Gel and Electrophoretic Methods

https://doi.org/10.14233/ajchem.2013.14250

Hassan Nosrati

Department of Mining and Metallurgical Engineering, Amirkabir University of Technology (Tehran Polytechnic), No. 424 Hafez Avenue, P.O. Box 15875-4413 Tehran, Iran

Mehran Shafi Hosseini

Department of Mining and Metallurgical Engineering, Amirkabir University of Technology (Tehran Polytechnic), No. 424 Hafez Avenue, P.O. Box 15875-4413 Tehran, Iran

Mohammad Nemati

Department of Wood and Paper Engineering, Science and Research Branch, Islamic Azad University, Tehran, Iran

Ahmad Samariha

Department of Wood and Paper Engineering, Science and Research Branch, Islamic Azad University, Tehran, Iran

Corresponding Author(s) : Hassan Nosrati

h.nosrati@gmail.com

Asian Journal of Chemistry, Vol. 25 No. 6 (2013): Vol 25 Issue 6
Article Published : January 9, 2013

Abstract

Nano-rods of titanium dioxide have been developed by electrophoretic deposition in polycarbonate templates with 180 nm diameter. Characteristics of the produced nanostructures have been investigated in terms of microstructure, morphology, phase composition, thermal behaviour and chemical bindings using scanning electron microscope, X-ray diffraction and Fourier transform infra red. Scanning electron microscope micrographs demonstrated that the TiO₂ nano-rods have grown completely directional with thoroughly similar diameter. In addition, X-ray diffraction analysis revealed that the developed nano-rods have yielded a mixture of anatine and rutile structures after annealing at 530 ºC for 50 min.

Keywords

Nano-rod Titanium dioxide Electrophoresis Sol-gel

Nosrati, H., Shafi Hosseini, M., Nemati, M., & Samariha, A. (2013). Production of TiO2 Nano-Rods Using Combination of Sol-Gel and Electrophoretic Methods. Asian Journal of Chemistry, 25(6), 3484–3486. https://doi.org/10.14233/ajchem.2013.14250

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References

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References

H. Jia, Z. Zheng, H. Zhao, L. Zhang and Z. Zou, Mater. Res. Bull., 44, 1312 (2009).

Y. Li, M. Guo, M. Zhang and X. Wang, Hydrothermal Synthesis and Characterization of TiO2 Nanorod Arrays on Glass Substrates (2009).

K. Pan, Q. Zhang, Q. Wang, Z. Liu, D. Wang, J. Li and Y. Bai, Thin Solid Films, 515, 4085 (2007).

K. Asagoe, S. Ngamsinlapasathian, Y. Suzuki and S. Yoshikawa, Cent. Eur. J. Chem., 5, 921 (2007).

X. Zhang, A. Jianhong, P. Lee, D.D. Sun and J.O. Leckie, J. Memb. Sci., 313, 44 (2008).

L. Francioso, A.M. Taurino, A. Forleo and P. Siciliano, Sens. Actuators B, 130, 70 (2008).

Z. Zhang, C. Wang, R. Zakaria and J.Y. Ying, J. Phys. Chem. B, 102, 10871 (1998).

Y. Wu, H. Yan, M. Huang, B. Messer, J.H. Song and P. Yang, Chem. Eur. J., 8, 1260 (2002).

S.K. Pradhan, P.J. Reucroft, F. Yang and A. Dozier, J. Crystal Growth, 256, 83 (2003).

A.M. Morales and C.M. Lieber, Science, 279, 208 (1998).

Y.X. Zhang, G.H. Li, Y.X. Jin, Y. Zhang, J. Zhang and L.D. Zhang, Chem. Phys. Lett., 365, 300 (2002).

A.S. Attar, M.S. Ghamsari, F. Hajiesmaeilbaigi, Sh. Mirdamadi, K. Katagiri and K. Koumoto, J. Mater. Sci., 43, 5924 (2008).

W. Wook, S. Park, K.J. Kim and C. Shin, J. Mater. Sci., 36, 4299 (2001).

T. Wen, J. Zhang, T.P. Chou, S.J. Limmer and G. Cao, J. Sol-Gel Sci. Technol., 33, 193 (2005).

H. Jia, Z. Zheng, H. Zhao, L. Zhang and Z. Zou, Mater. Res. Bull., 44, 1312 (2009).

W. Wook, S. Park, K.J. Kim and C. Shin, J. Matter. Sci., 36, 4299 (2001).

M.R. Mohammadi, M.C. Cordero-Cabrera, M. Ghorbani and D.J. Fray, J. Sol-Gel. Sci. Techn., 40, 15 (2006).

G. Cao, J. Phys. Chem., B108, 19921 (2004).

R.N. Basu, C.A. Randall and M.J. Mayo, J. Am. Ceram. Soc., 84, 33 (2001).

Vu Trung, M. Pavlik, N. Hebestreit and J. Pfleger, Electrochim. Acta, 51, 1117 (2005).

Issue

Vol. 25 No. 6 (2013): Vol 25 Issue 6

Production of TiO2 Nano-Rods Using Combination of Sol-Gel and Electrophoretic Methods

Corresponding Author(s) : Hassan Nosrati

Abstract

Keywords

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