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Synthesis and Characterization of Silver Oxide and Silver Chloride Nanoparticles with High Thermal Stability
Corresponding Author(s) : M. Rafiq H. Siddiqui
Asian Journal of Chemistry,
Vol. 25 No. 6 (2013): Vol 25 Issue 6
Abstract
In present studies, the synthesis of nanoparticles of silver oxide and silver chloride were carried out. The silver oxide nanoparticles were synthesized employing capping method while silver chloride nanoparticles were synthesized by simple precipitation of silver nitrate solution. Transmission Electron microscopic studies show that the size of silver oxide nanoparticles obtained is in the range of 2-10 nm while the size of silver chloride nanoparticles was found to be in the range of 2-12 nm. Silver chloride nanoparticles were found to be stable even at 650 ºC. Thermal studies suggest that silver chloride nanoparticles behave like ionic liquid or molten salt in the range of 455-650 ºC.
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References
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M. Zhang, S. Fang, A.A. Zakhidov, S.B. Lee, A.E. Aliev, C.D. Williams, K.R. Atkinson and R.H. Baughman, Science, 309, 1215 (2005).
A.R. Mayer and J.E. Mark, Colloid Polym. Sci., 275, 333 (1997).
M.H. Pishbin, A.R. Mohammadi and M. Nasri, Fuel Cells (Weinheim, Germany), 7, 291 (2007).
J.H. Lee, S.K. Hong and W.B. Ko, Asian J. Chem., 23, 5447 (2011).
K.I. Shimizu, K. Sugino, K. Sawabe and A. Satsuma, Chem. Eur. J., 15, 2341 (2009).
J.M. Schierholz, L.J. Lucas, A. Rump and G. Pulverer, J. Hosp. Infect., 40, 257 (1998).
S.H. Shin, M.K. Ye, H.S. Kim and H.S. Kang, Int. J. Immunopharmacol., 7, 1813 (2007).
C. Baker, A. Pradhan, L. Pakstis, D.J. Pochan and S.I. Shah, J. Nanosci. Nanotechnol., 5, 244 (2005).
J. Chen, C.M. Han, X.W. Lin, Z.J. Tang and S.J. Su, Zhonghua Wai Ke Za Zhi, 44, 50 (2006).
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C. Michael, US patent Feb 14, 2008 US 20080038630 A1 Application Mar 25, 2005 US 2005-90471.
A.I. Akimov and G.K. Savchuk, Inorg. Mater., 41, 542 (2005).
I. Tomoaki and A. Wakana, Japanese Patent May 19, 2005 JP 2005129407 A Application Oct 24, 2003 JP 2003-364886.
W. Xudong, W. Lei, Y. Yongzhe, Z. Liqing, C. Xing, W. Tao, L. Zhixia, X. Wei, M. Qianqiu, B. Xiaorong, S. Hisashi and F. Kennichi, Chinese patent May 20, 2009 CN 101435794 Application No.Dec 19, 2008CN 2008-10232735
C.N. Louis, K. Iyakutti and P. Malarvizhi, J. Phys. Condens. Mater, 16, 1577 (2004).
M. Yu, R. Skouta, L. Zhou, H.F. Jiang, X. Yao and C.J. Li, J. Org. Chem., 74, 3378 (2009).
P.K. Khanna, T.S. Kale, M. Shaikh, N.K. Rao and C.V.V. Satyanarayana, Mater. Chem. Phys., 110, 21 (2008).
M. Oliveira, D. Ugarte, D. Zanchet and A. Zarbin, J. Colloid Interf. Sci., 292, 429 (2005).
J. Bai, Y. Li, J. Du, S. Wang, J. Zheng, Q. Yang and X. Chen, Mater. Chem. Phys., 106, 412 (2007).
Y. Jinhu, Q. Limin, Z. Dongbai, M. Jiming and C. Humin, Cryst. Growth Design, 4, 1371 (2004).
M. Choi, K.H. Shin and J. Jang, J. Colloid Interf. Sci., 341, 83 (2010).
J.P. Tiwari and R.K. Chepuri, Solid State Ionics, 179, 299 (2008).
M. Hasan, I.V. Kozhevnikov, M.R. Siddiqui, A. Steiner and N. Winterton, Inorg. Chem., 38, 5637 (1999).
H.L. Jindal, Aust. J. Chem., 26, 57 (1973).
H. Maen, R. Eva and V. Juan, Langmuir, 19, 8467 (2003)