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Preparation and Characterization of Strontium Orthovanadate Nanoparticles by A Microwave-Assisted Solvothermal Method
Asian Journal of Chemistry,
Vol. 25 No. 5 (2013): Vol 25 Issue 5
Abstract
Strontium orthovanadate (Sr3V2O8) nanoparticles were synthesized successfully using a facile microwave solvothermal route followed by further heat-treatment. Well-crystallized Sr3V2O8 nanoparticles were formed after heat-treatment at 600 ºC for 3 h showing a fine and homogeneous morphology with particle sizes of 100-150 nm. The synthesized Sr3V2O8 nanoparticles were characterized by X-ray diffraction, Fourier transform infrared spectroscopy, scanning electron microscopy and transmission electron microscopy. The optical properties were investigated by photoluminescence emission and Raman spectroscopy.
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- T. Nakajima, M. Isobe, T. Tsuchiya, Y. Ueda and T. Kumagai, J. Luminescence, 129, 1598 (2009).
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- D. Wang, Z. Zou and J. Ye, Res. Chem. Intermed., 31, 433 (2005).
- M. Kurzawa, A. Blonska-Tabero, J. Therm. Anal. Calorim., 77, 17 (2004).
- P. Parhi and V. Manivannan, Mater. Res. Bull., 43, 2966 (2008).
- S.S. Kim, H. Ikuta and M. Wakihara, Solid State Ionics, 139, 57 (2001).
- P. Parhi, V. Manivannan, S. Kohli and P. Mccurdy, Bull. Mater. Sci., 31, 885 (2008).
- V. Manivannan, P. Parhi and J. Howard, J. Cryt. Growth, 310, 2793 (2008).
- R. Szymczak, M. Baran, J. Fink-Finowicki, B. Krzymanska, P. Aleshkevych, H. Szymczak, S.N. Barilo, G.L. Bychkov and S.V. Shiryaev, J. NonCryst. Solids, 354, 4186 (2008).
- S. Das, A.K. Mukhopadhyay, S. Datta and D. Basu, Bull. Mater. Sci., 32, 1 (2009).
- K.P.F. Siqueira, R.L. Moreira, M. Valadares and A. Dias, J. Mater. Sci., 45, 6083 (2010).
- J.C. Sczancoski, L.S. Cavalcante, M.R. Joya, J.A. Varela, P.S. Pizani and E. Longo, Chem. Eng. J., 140, 632 (2008).
- J. Bi, L. Wu, Z. Li, Z. Ding, X. Wang and X. Fu, J. Alloys Comp., 480, 684 (2009).
- T. Thongtem, A. Phuruangrant and S. Thongtom, Curr. Appl. Phys., 8, 189 (2008).
References
T. Nakajima, M. Isobe, T. Tsuchiya, Y. Ueda and T. Kumagai, J. Luminescence, 129, 1598 (2009).
F. Yen, R.P. Chaudhury, E. Galstyan, B. Lorenz, Y.Q. Wang, Y.Y. Sun and C.W. Chu, Physica B, 403, 1487 (2008).
N. Rogado, G. Lawes, D.A. Huse, A.P. Ramirez and R.J. Cava, Solid State Commun., 124, 229 (2002).
D. Wang, Z. Zou and J. Ye, Res. Chem. Intermed., 31, 433 (2005).
M. Kurzawa, A. Blonska-Tabero, J. Therm. Anal. Calorim., 77, 17 (2004).
P. Parhi and V. Manivannan, Mater. Res. Bull., 43, 2966 (2008).
S.S. Kim, H. Ikuta and M. Wakihara, Solid State Ionics, 139, 57 (2001).
P. Parhi, V. Manivannan, S. Kohli and P. Mccurdy, Bull. Mater. Sci., 31, 885 (2008).
V. Manivannan, P. Parhi and J. Howard, J. Cryt. Growth, 310, 2793 (2008).
R. Szymczak, M. Baran, J. Fink-Finowicki, B. Krzymanska, P. Aleshkevych, H. Szymczak, S.N. Barilo, G.L. Bychkov and S.V. Shiryaev, J. NonCryst. Solids, 354, 4186 (2008).
S. Das, A.K. Mukhopadhyay, S. Datta and D. Basu, Bull. Mater. Sci., 32, 1 (2009).
K.P.F. Siqueira, R.L. Moreira, M. Valadares and A. Dias, J. Mater. Sci., 45, 6083 (2010).
J.C. Sczancoski, L.S. Cavalcante, M.R. Joya, J.A. Varela, P.S. Pizani and E. Longo, Chem. Eng. J., 140, 632 (2008).
J. Bi, L. Wu, Z. Li, Z. Ding, X. Wang and X. Fu, J. Alloys Comp., 480, 684 (2009).
T. Thongtem, A. Phuruangrant and S. Thongtom, Curr. Appl. Phys., 8, 189 (2008).