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Vol. 25 No. 5 (2013): Vol 25 Issue 5

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A Solvothermal Process to Synthesize Calcium Metastannate Nanoparticles Assisted by Microwave Irradiation

https://doi.org/10.14233/ajchem.2013.CSLimC
Chang Sung Lim
Department of Advanced Materials Science & Engineering, Hanseo University, Seosan 356-706, South Korea

Corresponding Author(s) : Chang Sung Lim

cslim@hanseo.ac.kr

Asian Journal of Chemistry, Vol. 25 No. 5 (2013): Vol 25 Issue 5

Abstract

Calcium metastannates (CaSnO3) nanoparticles were synthesized successfully using a facile microwave solvothermal route followed by further heat-treatment. Well-crystallized CaSnO3 nanoparticles were formed after heat-treatment at 800 ºC for 3 h showing a fine and homogeneous morphology with particle sizes of 20-40 nm. The synthesized CaSnO3 nanoparticles were characterized by X-ray diffraction, Fourier transform infrared spectroscopy, scanning electron microscopy, energy-dispersive X-ray spectroscopy and transmission electron microscopy.

Keywords

Calcium metastannates Microwave irradiation Solvothermal process Nanoparticles
Sung Lim, C. (2012). A Solvothermal Process to Synthesize Calcium Metastannate Nanoparticles Assisted by Microwave Irradiation. Asian Journal of Chemistry, 25(5), 2418–2420. https://doi.org/10.14233/ajchem.2013.CSLimC
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