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Synthesis, Crystal Structure and Antibacterial Activity of Ca(II) Complex with 2-(Phenylsulfonamido)acetic Acid
Corresponding Author(s) : Tai Xi-Shi
Asian Journal of Chemistry,
Vol. 25 No. 4 (2013): Vol 25 Issue 4
Abstract
A new ligand 2-(phenylsulfonamido)acetic acid (L) and its Ca(II) complex have been synthesized and characterized by elemental analysis, IR spectroscopy and single-crystal X-ray diffraction. The results showed that the complex formed one dimensional chained structure through intramolecule and intermolecule hydrogen bonds and p-p stacking. The antibacterial assay of the Ca(II) complex and the lignd L was tested using a modified version of 2-fold serial dilution method. The Ca(II) complex shows considerable antibacterial activity against Escherichia coli, Bacillus subtilis and Staphylococcus white.
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- X.S. Tai, Y.M. Feng, F.Y. Kong, D.Q. Wang and M.Y. Tan, Chin. J. Inorg. Chem., 24, 831 (2008).
- Y. Su, S.Q. Zang, C.L. Ni, Y. Z. Li and Q.J. Meng, Chin. J. Inorg. Chem., 20, 845 (2004).
- S. Gao, Z.Y. Zhang, L.H. Huo, H. Zhao and J.G. Zahao, Chin. J. Inorg. Chem., 21, 771 (2005).
- Y. Lu, G.C. Deng, F.M. Miao and Z.M. Li, J. Inorg. Biochem., 96, 487 (2003).
- S.M. Avaeva, N.N. Vorobyeva, S.A. Kurilova, T.I. Nazarova, K.M. Polyakov, E.V. Rodina and V.R. Samygina, Biochemistry, 65, 442 (2000).
- X.S. Tai, J. Yin, Y.M. Feng and F.Y. Kong, Chin. J. Inorg. Chem., 23, 1812 (2007).
- W.K. Cao, S.X. He, J.S. Zhao, R. Yang, Q.Z. Shi, D.Q. Wang and J.M. Dou, Acta Chim. Sin., 61, 1612 (2003).
- B. Chen, M. Eddaoudi, S.T. Hyde, M.O'Keeffe and O.M. Yaghi, Science, 291, 1021 (2001).
- S.F. Brady and J. Clardy, J. Am. Chem. Soc., 122, 12903 (2000).
- B. Zhao, P. Cheng, X.X. Chen, C. Cheng, W. Shi, D.Z. Liao, S.P. Yan and Z.H. Jiang, J. Am. Chem. Soc., 126, 3012 (2004).
- Y.Y. Yang, M.H. Zeng, S.H. Zhang and H. Liang, Struct. Chem., 19, 771 (2008).
- B.S. Haman and S. Sagdinc, Struct. Chem., 19, 381 (2008).
- L.J. Tian, H.J. Yang, X.L. Zheng, Z.H. Ni, D.M. Yan, L.L. Tu and J.Z. Jiang, Appl. Organometal. Chem., 23, 24 (2009).
- Y.H. Wen, X. Feng, Y.L. Feng, Y.Z. Lan and Y.G. Yao, Inorg. Chem. Commun., 11, 659 (2008).
- G.M. Sheldrick, SHELXL-97, Program for Crystal Structure Solution; University of GÖttingen: GÖttingen, Germany (1997).
- G.M. Sheldrick, SHELXTL-97, Program for Crystal Structure Solution; University of GÖttingen: GÖttingen, Germany (1997).
- J.L. Zhou, Q.S. Yao and H. Xu, Chin. J. Modern Appl. Pharm., 17, 148 (2000).
- K. Nakamoto, Infrared and Ramen Spectra of Inorganic and Coordination Compounds, New York: John Wiley and Sons, American, edn. 3 (1978).
- X.S. Tai, Adv. Mater. Res., 282-283, 108 (2011).
References
X.S. Tai, Y.M. Feng, F.Y. Kong, D.Q. Wang and M.Y. Tan, Chin. J. Inorg. Chem., 24, 831 (2008).
Y. Su, S.Q. Zang, C.L. Ni, Y. Z. Li and Q.J. Meng, Chin. J. Inorg. Chem., 20, 845 (2004).
S. Gao, Z.Y. Zhang, L.H. Huo, H. Zhao and J.G. Zahao, Chin. J. Inorg. Chem., 21, 771 (2005).
Y. Lu, G.C. Deng, F.M. Miao and Z.M. Li, J. Inorg. Biochem., 96, 487 (2003).
S.M. Avaeva, N.N. Vorobyeva, S.A. Kurilova, T.I. Nazarova, K.M. Polyakov, E.V. Rodina and V.R. Samygina, Biochemistry, 65, 442 (2000).
X.S. Tai, J. Yin, Y.M. Feng and F.Y. Kong, Chin. J. Inorg. Chem., 23, 1812 (2007).
W.K. Cao, S.X. He, J.S. Zhao, R. Yang, Q.Z. Shi, D.Q. Wang and J.M. Dou, Acta Chim. Sin., 61, 1612 (2003).
B. Chen, M. Eddaoudi, S.T. Hyde, M.O'Keeffe and O.M. Yaghi, Science, 291, 1021 (2001).
S.F. Brady and J. Clardy, J. Am. Chem. Soc., 122, 12903 (2000).
B. Zhao, P. Cheng, X.X. Chen, C. Cheng, W. Shi, D.Z. Liao, S.P. Yan and Z.H. Jiang, J. Am. Chem. Soc., 126, 3012 (2004).
Y.Y. Yang, M.H. Zeng, S.H. Zhang and H. Liang, Struct. Chem., 19, 771 (2008).
B.S. Haman and S. Sagdinc, Struct. Chem., 19, 381 (2008).
L.J. Tian, H.J. Yang, X.L. Zheng, Z.H. Ni, D.M. Yan, L.L. Tu and J.Z. Jiang, Appl. Organometal. Chem., 23, 24 (2009).
Y.H. Wen, X. Feng, Y.L. Feng, Y.Z. Lan and Y.G. Yao, Inorg. Chem. Commun., 11, 659 (2008).
G.M. Sheldrick, SHELXL-97, Program for Crystal Structure Solution; University of GÖttingen: GÖttingen, Germany (1997).
G.M. Sheldrick, SHELXTL-97, Program for Crystal Structure Solution; University of GÖttingen: GÖttingen, Germany (1997).
J.L. Zhou, Q.S. Yao and H. Xu, Chin. J. Modern Appl. Pharm., 17, 148 (2000).
K. Nakamoto, Infrared and Ramen Spectra of Inorganic and Coordination Compounds, New York: John Wiley and Sons, American, edn. 3 (1978).
X.S. Tai, Adv. Mater. Res., 282-283, 108 (2011).