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Growth, Structural, Spectral, Optical and Mechanical Studies of Calcium Mixed Strontium Tartrate Single Crystals
Corresponding Author(s) : M. Mary Freeda
Asian Journal of Chemistry,
Vol. 25 No. 4 (2013): Vol 25 Issue 4
Abstract
Calcium mixed strontium tartrate crystals were grown by controlled diffusion in silica gel at ambient temperature. Structural characterization of the grown crystals was carried out by single crystal and powder X-ray diffraction analysis. The functional groups present in the crystals were identified using Fourier transform infrared spectral analysis. The chemical composition of the sample was verified using EDAX spectrum. The nonlinear optical property of the grown crystal was confirmed by Kurtz-Perry powder technique. The UV-VIS-NIR transmission spectrum was recorded to study the optical transparency of the grown crystal. Mechanical strength of the grown crystals was analyzed by Vicker's microhardness test.
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- X. Sahaya Shajan and C. Mahadevan, Cryst. Res. Technol., 40, 598 (2005).
- M.H. Rahimkutty, K.R. Babu, K.S. Pillai, M.R.S. Kumar and C.M.K. Nair, Bull. Mater. Sci., 24, 249 (2001).
- S.K. Arora, V. Patel, B. Chudasama and B. Amin, J. Cryst. Growth, 275, e657 (2005).
- A. Firdous, I. Quasim, M.M. Ahmad and P.N. Kotru, Cryst. Res. Technol., 43, 1015 (2008).
- F.J. Rethinam, D. Arivuoli, S. Ramasamy and P. Ramasamy, Cryst. Res. Technol., 28, 861 (1993).
- B. Gowri and X.S. Shajan, Mater. Lett., 60, 1338 (2006).
- K. Suryanarayana and S.M. Dharmaprakash, J. Phys. Chem. Solids, 58, 1599 (1997).
- H.K. Henisch, Crystal Growth in Gels, Dover Publications Inc., New York, p. 20 (1996).
- S.K. Kurtz and T.T. Perry, J. Appl. Phys., 39, 3798 (1968).
- K.K. Rao, V. Surender and B.S. Rani, Bull. Mater. Sci., 25, 641 (2002).
- T. Balakrishnan and K. Ramamurthi, Mater. Lett., 62, 65 (2008).
- J.B. Charles and F.D. Gnanam, J. Mater. Sci. Lett., 12, 1395 (1993).
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References
G.A. Kiosse, In ed.: T.I. Malinowskii, In Crystal Structure of Inorganic Compounds, (Shtuntsa Press, Kishineve), p. 103 (1974).
H.B. Gon, J. Cryst. Growth, 102, 501 (1990).
S.K. Arora, V. Patel, B. Amin and A. Kothari, Bull. Mater. Sci., 27, 141 (2004).
V.S. Yadava and V.M. Padmanabhan, Acta Cryst. B, 29, 493 (1973).
C.C. Desai and A.H. Patel, Bull. Mater. Sci., 11, 31 (1988).
M.V. Hobden, J. Appl. Phys., 38, 4365 (1967).
S.S. Sekarapandian, K. Vivekanandan and P. Kolandaivel, Cryst. Res. Technol., 34, 873 (1996).
S.K. Arora, V. Patel, A. Kothari and B. Chudasama, Mater. Sci. Eng. B, 113, 263 (2004).
C. Medrano, P. Gunter and H. Arend, Phys. Status Solidi, 14B, 749 (1987).
P. Selvarajan, B.N. Das, H.B. Gon and K.V. Rao, J. Mater. Sci. Lett., 12, 1210 (1993).
S.R. Suthar and M.J. Joshi, Cryst. Res. Technol., 41, 664 (2006).
M.E. Torres, T. Lopez, J. Stockel, X. Solans, M. Garcia-Valles, E. RodriguezCastellon and C. Gonzalez-Silingo, J. Solid State Chem., 163, 491 (2002).
X. Sahaya Shajan and C. Mahadevan, Cryst. Res. Technol., 40, 598 (2005).
M.H. Rahimkutty, K.R. Babu, K.S. Pillai, M.R.S. Kumar and C.M.K. Nair, Bull. Mater. Sci., 24, 249 (2001).
S.K. Arora, V. Patel, B. Chudasama and B. Amin, J. Cryst. Growth, 275, e657 (2005).
A. Firdous, I. Quasim, M.M. Ahmad and P.N. Kotru, Cryst. Res. Technol., 43, 1015 (2008).
F.J. Rethinam, D. Arivuoli, S. Ramasamy and P. Ramasamy, Cryst. Res. Technol., 28, 861 (1993).
B. Gowri and X.S. Shajan, Mater. Lett., 60, 1338 (2006).
K. Suryanarayana and S.M. Dharmaprakash, J. Phys. Chem. Solids, 58, 1599 (1997).
H.K. Henisch, Crystal Growth in Gels, Dover Publications Inc., New York, p. 20 (1996).
S.K. Kurtz and T.T. Perry, J. Appl. Phys., 39, 3798 (1968).
K.K. Rao, V. Surender and B.S. Rani, Bull. Mater. Sci., 25, 641 (2002).
T. Balakrishnan and K. Ramamurthi, Mater. Lett., 62, 65 (2008).
J.B. Charles and F.D. Gnanam, J. Mater. Sci. Lett., 12, 1395 (1993).
E.M. Onitsch, Mikroskopie, 2, 131 (1947).