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Synthesis and Crystal Structure of Terephthalaldehyde-bis-(thiosemicarbazone)-bis-(dimethyl sulfoxide) Solvate
Corresponding Author(s) : Peiyuan Li
Asian Journal of Chemistry,
Vol. 25 No. 4 (2013): Vol 25 Issue 4
Abstract
A thiosemicarbazone single crystal synthesized with a formula as C10H12N6S2·2C2H6OS, was synthesized by 1,4-phthalaldehyde and 4-methylthiosemicarbazide. The crystal is triclinic, space group P-1 with unit cell parameters: a = 5.9519(5) Å, b = 7.4721(7) Å, c = 12.5450(13), a = 77.348(8)º, b = 78.672(8)º, g = 79.193(7)º, V = 527.64(8) Å3, Z = 1, Mr = 436.63, Dc = 1.374 g/cm3, μ = 0.471 mm-1, F(000) = 230, R = 0.0844, wR = 0.2607 for 1902 reflections with I > 2s (I).
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- T.S. Lobana, G. Bawa, R.J. Butcher and C.W. Liu, Z. Anorg. Allg. Chem., 635, 355 (2009).
- R. Pingaew, S. Prachayasittikul and S. Ruchirawat, Molecules, 15, 988 (2010).
- T.S. Lobana, G. Bawa and R.J. Butcher, Inorg. Chem., 47, 1488 (2008).
- K. Lee, P. Thanigaimalai, V.K. Sharma, M. Kim, E. Roh, B. Hwang, Y. Kim and S. Jung, Bioorg. Med. Chem. Lett., 20, 6794 (2010).
References
T.S. Lobana, G. Bawa, R.J. Butcher and C.W. Liu, Z. Anorg. Allg. Chem., 635, 355 (2009).
R. Pingaew, S. Prachayasittikul and S. Ruchirawat, Molecules, 15, 988 (2010).
T.S. Lobana, G. Bawa and R.J. Butcher, Inorg. Chem., 47, 1488 (2008).
K. Lee, P. Thanigaimalai, V.K. Sharma, M. Kim, E. Roh, B. Hwang, Y. Kim and S. Jung, Bioorg. Med. Chem. Lett., 20, 6794 (2010).