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Crystal Structure and Luminescent Properties of Supramolecular Compound [C12H12N2]2+[C16H8O10S]2-
Corresponding Author(s) : Feng Fu
Asian Journal of Chemistry,
Vol. 25 No. 3 (2013): Vol 25 Issue 3
Abstract
A new supramolecular compound [C12H12N2]2+[C16H8O10S]2- was synthesized and characterized by elemental analysis, IR and single-crystal X-ray diffraction. In the crystal structure, multiform hydrogen bonds (N-H···O and C-H···O) lead to a three-dimensional supramolecular architecture. The luminescent properties of the compound in the solid state were investigated. The crystal be longs to monoclinic, space group C2/c, a = 3.039(3), b = 0.48803(7), c = 2.0251(2) nm, b = 100.319(2)º, Z = 4, V = 2.955(3) nm3, R1 = 0.0664 and wR2 = 0.1637 (CCDC 754951).
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References
K.T. Holman, S.M. Martin, D.P. Parker and M.D. Ward, J. Am. Chem. Soc., 123, 4421 (2001).
X.L. Zhang and X.M. Chen, Cryst. Growth Des., 5, 617 (2005).
D.J. Plaut, K.M. Lund and M.D. Ward, Chem. Commun., 769 (2000).
Z.X. Du, M.L. Han, J.G. Wang and J.H. Qin, Z. Kristallogr. NCS, 221, 499 (2006).
Y.J. Wang and L.M. Tang, Progr. Chem., 18, 308 (2006).
M. Du, Z.H. Zhang and X.J. Zhao, Cryst. Growth Des., 5, 1199 (2005).
SHELXTL 6.10, Bruker Analytical Instrumentation, Madison, Wisconsin, USA (2000).
A.L. Spek, J. Appl. Cryst., 36, 7 (2003).
A.L. Spek, PLATON[cp], Version of March, University of Utrecht, The Netherlands (2004).
W.W. Dong, D.S. Li, J. Zhao, L. Tang and X.Y. Hou, Acta Crystallogr., E64, o2252 (2008)