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Vol. 25 No. 2 (2013): Vol 25 Issue 2

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Synthesis and Crystal Structure of [µ2-1,1'-(1,4-Butanediyl)-bis-(imidazole)(µ2-oxalato)Zn(II)]

https://doi.org/10.14233/ajchem.2013.13224
Guangyin Wang
Key Laboratory of Coordination Chemistry and Functional Materials in Universities of Shandong (Dezhou University), Department of Chemistry, Dezhou University, Shandong 253023, P.R. China

Corresponding Author(s) : Guangyin Wang

dzgywang@126.com

Asian Journal of Chemistry, Vol. 25 No. 2 (2013): Vol 25 Issue 2

Abstract

Hydrothermal reactions of 1,1'-(1,4-butanediyl)-bis-(imidazole) (bbi) and oxalic acid (ox) with zinc nitrate gave rise to one new coordination polymer, namely, [Zn(bbi)(ox)]n. It was characterized by elemental analysis and single-crystal X-ray diffraction methods. This compound has one Zn metal center and shows a 3D three-fold interpenetrating framework, leaving no void to host the solvent molecules.

Keywords

Hydrothermal synthesis Coordination polymer Crystal structure
Wang, G. (2012). Synthesis and Crystal Structure of [µ2-1,1’-(1,4-Butanediyl)-bis-(imidazole)(µ2-oxalato)Zn(II)]. Asian Journal of Chemistry, 25(2), 1171–1172. https://doi.org/10.14233/ajchem.2013.13224
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References
  1. H.K. Wong, H. Yeung, W. Lee and W.T. Wong, Chem. Commun., 4841 (2006).
  2. T.J. Burchell, D.J. Eisler and R.J. Puddephatt, Inorg. Chem., 43, 5550 (2004).
  3. A. El-Dissouky, O. Al-Fulaij, M.K. Awad and S. Rizk, J. Coord. Chem., 63, 330 (2010).
  4. C.-C. Wang and P. Wang, Asian J. Chem., 24, 425 (2012).
  5. S.H. Zhang, N. Li, C.M. Ge, C. Feng and L.F. Ma, Dalton Trans., 40, 3000 (2011).
  6. D.F. Sun, D.J. Collins, Y.X. Ke and H.C. Zhou, Chem. Eur. J., 12, 3768 (2006).
  7. M. Eddaoudi, D.B. Moler, H.L. Li, B.L. Chen, T.M. Reineke, M. O'Keeffe and O.M. Yaghi, Acc. Chem. Res., 34, 319 (2001).
  8. D.F. Weng, Z.M. Wang and S. Gao, Chem. Soc. Rev., 40, 3157 (2011).
  9. L.F. Ma, Q.L. Meng, L.Y. Wang, B. Liu and F.P. Liang, Dalton Trans., 39, 8210 (2010).
  10. S. Ma and H.-C. Zhou, J. Am. Chem. Soc., 128, 11734 (2006).
  11. B.L. Wu, P. Zhang, Y.Y. Niu, H.Y. Zhang, Z.J. Li and H.W. Hou, Inorg. Chim. Acta, 361, 2203 (2008).
  12. T.L. Hu, R.Q. Zou, J.R. Li and X.H. Bu, Dalton Trans., 1302 (2008).
  13. Bruker, Smart and Saint, Bruker AXS Inc., Madison, Wisconsin, USA (2007).
  14. Bruker, Sadabs, Bruker AXS Inc., Madison, Wisconsin, USA (2001).
  15. A. Altomare, M.C. Burla, M. Camalli, G.L. Cascarano, C. Giacovazzo, A. Guagliardi, A.G.G. Moliterni, G. Polidori and R. Spagna, J. Appl. Cryst., 32, 115 (1999).
  16. G.M. Sheldrick, Acta Cryst., A64, 112 (2008).
  17. L.J. Farrugia, J. Appl. Cryst., 32, 837 (1999).
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