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Direct Room-Temperature Synthesis of Organic-Inorganic Hybrid MCM-48 Nanoparticles
Corresponding Author(s) : Xiaolai Wang
Asian Journal of Chemistry,
Vol. 25 No. 10 (2013): Vol 25 Issue 10
Abstract
A series of organic-inorganic hybrid MCM-48 materials were directly synthesized by a rapid and facile way at room temperature without employing hydrothermal synthesis for the first time. The resultant samples were characterized through XRD, N2 adsorption/desorption, FT-IR, FESEM and HRTEM. The characterization results revealed that all the samples with typical mesoporous structure were successfully modified by the introduced organic groups.
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References
S. Fujita and S. Inagaki, Chem. Mater., 20, 891 (2008).
M.C. Burleigh, M.A. Markowitz, S. Jayasundera, M.S. Spector, C.W. Thomas and B.P. Gaber, J. Phys. Chem. B, 107, 12628 (2003).
C.T. Kresge, M.E. Leonowicz, W.J. Roth, J.C. Vartuli and J.S. Beck, Nature, 359, 710 (1992).
J.S. Beck, J.C. Vartuli, W.J. Roth, M.E. Leonowicz, C.T. Kresge, K.D. Schmitt, C.T.W. Chu, D.H. Olson and E.W. Sheppard, J. Am. Chem. Soc., 114, 10834 (1992).
K. Schumacher, C. du F. von Hohenesche, K.K. Unger, R. Ulrich, A. D. Chesne, U. Wiesner and H.W. Spiess, Adv. Mater., 11, 1194 (1999).
B. Boote, H. Subramanianb and K.T. Ranjit, Chem. Commun., 4543 (2007).
F.O.M. Gaslain, C. Delacote, A. Walcarius and B. Lebeau, J. Sol-Gel. Sci. Technol., 49, 112 (2009).
A. Matsumoto, K. Tsutsumi, K. Schumacher and K.K. Unger, Langmuir, 18, 4014 (2002).
E.F. Vansant, P. Van Der Voort and K.C. Vrancken, Stud. Surf. Sci. Catal., 93, 59 (1995).
R.M. Silverstein, G.C. Bassler and T.C. Morril, Spectroscopic Identification of Organic Compounds, Wiley, New York, Chap. 2, edn. 5, (1991).