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Synthesis of Platinum Nanoparticles Conjugates of Ceftriaxone and its Schiff Bases Using Sodium Borohydride and Trisodium Citrate
Corresponding Author(s) : Ahlam Jameel Abdulghani
Asian Journal of Chemistry,
Vol. 29 No. 2 (2017): Vol 29 Issue 2
Abstract
The synthesis of platinum nanoparticles conjugates was achieved by the reduction of hexachloroplatinic acid with sodium borohydride (NaBH4) and trisodium citrate in aqueous solutions using ceftriaxone and two Schiff base ligands derived from ceftriaxone sodium with 1H-indole-2,3-dione (isatin), L1 and 1-acetyl indoline-2,3-dione (N-acetylisatin) L2 as capping agents. The synthesized platinum nanoparticles were characterized by UV-visible spectrophotometry, X-ray diffraction, scanning electron microscope and atomic force microscope analysis. Conjugation of the ligands with the nanoparticles was characterized by FT-IR spectrophotometry.
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- F. Li, F. Li, J. Song, J. Song, D. Han and L. Niu, Electrochem. Commun., 11, 351 (2009).
- W. Yang, Y. Ma, J. Tang and X. Yang, Colloids Surf. A, 302, 628 (2007).
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- A.J. Abdulghani and S.K. Mohuee, J. Chem. Biol. Phys. Sci., Section A: Chem. Sci., 6, 579 (2016).
- A. Bragaru, M. Miu, M. Simion, A. Iordanescu, M. Danila, A. Radoi and A. Dinescu, Rom. J. Inf. Sci. Technol., 13, 350 (2010).
- A.J. Martins, M. Benelmekki, V. Teixeira and P.J.G. Coutinho, J. Nano Res., 18-19, 97 (2012).
- J.W. Guo, T.S. Zhao, J. Prabhuram and C.W. Wong, Electrochim. Acta, 50, 1973 (2005).
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References
D. Kwak, Y. Lee, K. Lee, A. Park, J. Moon and K. Park, Int. J. Electrochem. Sci., 8, 5102 (2013).
D. Li and S. Komarneni, Z. Naturforsch., 61b, 1566 (2006).
E. Gharibshahi and E. Saion, Int. J. Mol. Sci., 13, 14723 (2012).
V. Nguyen, M. Ohtaki, V. Ngo, M. Cao and M. Nogami, Adv. Nat. Sci.: Nanosci. Nanotechnol., 3, 025005 (2012).
Y. Li, S.-M. Chen, W.-C. Chen, Y.-S. Li, M.A. Ali and F.M.A. AlHemaid, Int. J. Electrochem. Sci., 6, 6398 (2011).
F. Li, F. Li, J. Song, J. Song, D. Han and L. Niu, Electrochem. Commun., 11, 351 (2009).
W. Yang, Y. Ma, J. Tang and X. Yang, Colloids Surf. A, 302, 628 (2007).
G.S. Devi and V.J. Rao, Bull. Mater. Sci., 23, 467 (2000).
A.J. Abdulghani and S.K. Mohuee, J. Chem. Biol. Phys. Sci., Section A: Chem. Sci., 6, 579 (2016).
A. Bragaru, M. Miu, M. Simion, A. Iordanescu, M. Danila, A. Radoi and A. Dinescu, Rom. J. Inf. Sci. Technol., 13, 350 (2010).
A.J. Martins, M. Benelmekki, V. Teixeira and P.J.G. Coutinho, J. Nano Res., 18-19, 97 (2012).
J.W. Guo, T.S. Zhao, J. Prabhuram and C.W. Wong, Electrochim. Acta, 50, 1973 (2005).
A. Monshi, M.R. Foroughi and M.R. Monshi, World J. Nano Sci. Eng., 2, 154 (2012).