Synthesis of 2-Substiuted-5,5-dimethyl-1,3,2-dioxa-phosphorinane-2-Oxides
Corresponding Author(s) : C. Devendranath Reddy
Asian Journal of Chemistry,
Vol. 8 No. 1 (1996): Vol 8 Issue 1
Abstract
The equimolar reaction of 2,2,-dimethyl-1,3-propanediol with
phosphorus oxychloride afforded the monochloride, 2-chloro-
5,5-dimethyl-1,3,2-dioxaphosphorinane 2-oxide which was subsequently
reacted with various thiols and amines to yield a series
of 2-thiophenyl /thioalkyl /aIkylamino-5,5-dimethyl-1,3,2-dioxaphos
phorinane-2-oxides. Their structures were confinned by elemental
analyse, IR, 1H, 31P NMR and mass spectra.
Keywords
Synthesis
2-Substiuted-5,5-dimethyl-1,3,2-dioxa-phosphorinane-2-Oxides
Raghu, K., Devendranath Reddy, C., & Naga Raju, C. (2010). Synthesis of 2-Substiuted-5,5-dimethyl-1,3,2-dioxa-phosphorinane-2-Oxides. Asian Journal of Chemistry, 8(1), 45–48. Retrieved from https://asianpubs.org/index.php/ajchem/article/view/24017
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