Thermal and Powder X-ray Diffraction Studies of Copper(II) Complexes of Schiff Bases

P.G. More; R.B. Bhalvankar

Issue

Vol. 13 No. 4 (2001): Vol 13 Issue 4

Issue Published : October 10, 2001

Thermal and Powder X-ray Diffraction Studies of Copper(II) Complexes of Schiff Bases

P.G. More

Department of Chemistry, Shivaji University, P.G., Centre, Solapur-414 003, India

R.B. Bhalvankar

Department of Chemistry, Shivaji University, P.G., Centre, Solapur-414 003, India

Corresponding Author(s) : P.G. More

Asian Journal of Chemistry, Vol. 13 No. 4 (2001): Vol 13 Issue 4
Article Published : March 30, 2010

Abstract

Copper(II) complexes (CuL₂) of the Schiff bases (LH) derived
from 4-phenyl-2-aminothiazole and o-hydroxyaldehydes have been,
characterized by thermogravimetric analysis and powder X-ray diffraction
studies. The TG curves are critically analysed to evaluate
the various methods such as Freeman-Carroll, Coats-Redfern, MacCallum-
Tanner, Horowitz-Metzger and Zsako. The values of kinetic
parameters calculated by these methods are in good mutual agreement.
A tetragonal crystal system is proposed on the basis of X-ray
diffraction studies. Various X-ray parameters (lattice parameters,
volume of unit cell and particle size) are calculated.

Keywords

Thermal Powder X-ray Diffraction Study Cu(II) Schiff bases

More, P., & Bhalvankar, R. (2010). Thermal and Powder X-ray Diffraction Studies of Copper(II) Complexes of Schiff Bases . Asian Journal of Chemistry, 13(4), 1484–1488. Retrieved from https://asianpubs.org/index.php/ajchem/article/view/22829

Issue

Vol. 13 No. 4 (2001): Vol 13 Issue 4

Thermal and Powder X-ray Diffraction Studies of Copper(II) Complexes of Schiff Bases

Corresponding Author(s) : P.G. More

Abstract

Keywords

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