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Vol. 18 No. 3 (2006): Vol 18 Issue 3

Synthesis and X-ray Structure of a Novel N´ -Ferrocenylmethyl-N´ -phenylbenzohydrazide

B. Terki
VPRS Laboratory, University of Ouargla, B.P. No. 511, Ouargla-30000, Algeria
T. Lanez
VPRS Laboratory, University of Ouargla, B.P. No. 511, Ouargla-30000, Algeria
S. Belaidi
VPRS Laboratory, University of Ouargla, B.P. No. 511, Ouargla-30000, Algeria
H. Gornitzka
VPRS Laboratory, University of Ouargla, B.P. No. 511, Ouargla-30000, Algeria
A. Ourari
VPRS Laboratory, University of Ouargla, B.P. No. 511, Ouargla-30000, Algeria

Corresponding Author(s) : T. Lanez

clanez@yahoojr

Asian Journal of Chemistry, Vol. 18 No. 3 (2006): Vol 18 Issue 3

Abstract

Reaction of ferrocenylmethyltrimethylammonium iodide with N´-phenylbenzohydrazide afforded a novel stable N´-ferrocenylmethyl-N´-phenylbenzohydrazide which was characterized by 1H and 13C NMR, mass spectroscopy and X-ray crystallography. The product crystallizes in the orthorhombic space group Pbca. The structure analysis confirms the optimized geometry obtained by molecular modelling calculations. The electrochemical behaviour of the N´-ferrocenylmethyl-N´-phenylbenzohydrazide derivative has been studied by cyclic voltammetry.

Keywords

a Ferrocene N'-rerrocenylrnethyl-N'.phenylbenzohydrazide X-ray crystal structure Molecular modelling Cyclic voltammetry
(1)
Terki, B.; Lanez, T.; Belaidi, S.; Gornitzka, H.; Ourari, A. Synthesis and X-Ray Structure of a Novel N´ -Ferrocenylmethyl-N&Acute; -Phenylbenzohydrazide. ajc 2010, 18, 2074-2080.
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