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Vol. 32 No. 8 (2020): Vol 32 Issue 8, 2020

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Synthesis of Dimethyl Octahydroquinazolinones by using Electrochemically Prepared Copper Oxide Nanoparticles

https://doi.org/10.14233/ajchem.2020.22704
Manisha R. Sawant
Department of Chemistry, New Arts, Commerce and Science College, Ahmednagar-414001, India
Suresh T. Gaikwad
Department of Chemistry, Babasaheb Ambedkar Marathwada University, Aurangabad-431004, India
Bhaskar H. Zaware
Department of Chemistry, New Arts, Commerce and Science College, Ahmednagar-414001, India
Anjali S. Rajbhoj
Department of Chemistry, Babasaheb Ambedkar Marathwada University, Aurangabad-431004, India

Corresponding Author(s) : Manisha R. Sawant

sawantmr22@gmail.com

Asian Journal of Chemistry, Vol. 32 No. 8 (2020): Vol 32 Issue 8, 2020

Abstract

Present work involves the synthesis of substituted dimethyl octahydroquinazolinones by using electrochemically prepared copper oxide nanoparticles as catalyst in microwave. Copper oxide  nanoparticles were prepared in appreciable yield by using electrochemical reduction method of synthesis in the presence of tetrabutylphosphonium bromide for capping. The prepared  nanoparticles were analyzed by UV, FTIR, TGA, X-ray diffraction and electron microscopic studies. The nanoparticles of copper oxide then were successfully used as a catalyst in multicomponent reaction between diketones, substituted aldehydes and urea/thiourea to synthesize substituted dimethyl octahydroquinazolinones.

Keywords

Electrochemical reduction Copper oxide nanoparticles Tetrabutylphosphonium bromide Octahydroquinazolinones
Sawant, M. R. ., Gaikwad, S. T. ., Zaware, B. H. ., & Rajbhoj, A. S. . (2020). Synthesis of Dimethyl Octahydroquinazolinones by using Electrochemically Prepared Copper Oxide Nanoparticles. Asian Journal of Chemistry, 32(8), 1895–1902. https://doi.org/10.14233/ajchem.2020.22704
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