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Indirect Determination of Manganese in Its Slag by Atomic Fluorescence Spectrometry
Corresponding Author(s) : Jian-Ping Lu
Asian Journal of Chemistry,
Vol. 26 No. 18 (2014): Vol 26 Issue 18
Abstract
A novel method, based on that when the manganese in its slag was enriched and separated by a water soluble polymer, polypropylene pyrrolidone, the standard As(III), which was added, reduced the manganese in a 0.3 mol/L sulfuric acid medium, and the excess As(III) was determined on behalf of manganese, is established for indirect determination of manganese by hydride generation-atomic fluorescence spectrometry. Under optimum conditions, manganese content in 0-16 μg/L showed a good linear relationship. The detection limit was 0.0091 μg/mL. The method was applied to determine the manganese in its slag with a satisfactory result.
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- X.-L. Yang, G.-L. Wang and Z.-C. Chang, Med. Recapitulate, 12, 1134 (2006)..
- M.-P. Sassine, D. Mergler, R. Bowler and H.K. Hudnell, Soc. Biol. Psychiatry, 51, 909 (2002); doi:10.1016/S0006-3223(01)01350-6.
- J.J. Jing and J.M. Xie, Guangdong Trace Elem. Sci., 15, 6 (2008).
- M.-M. Lu, Equip. Manufact. Technol., 5, 22 (2008).
- J.S. Roitz and K.W. Bruland, Anal. Chim. Acta, 344, 175 (1997); doi:10.1016/S0003-2670(97)00041-X.
- J. Mierzwa, Y.-C. Sun and M.-H. Yang, Spectrochim. Acta B, 53, 63 (1998); doi:10.1016/S0584-8547(97)00119-5.
- N. Tokman, J. Hazard. Mater., 143, 87 (2007); doi:10.1016/j.jhazmat.2006.08.068.
- F. Sabermahani and M.A. Taher, Anal. Chim. Acta, 565, 152 (2006); doi:10.1016/j.aca.2006.02.048.
References
X.-L. Yang, G.-L. Wang and Z.-C. Chang, Med. Recapitulate, 12, 1134 (2006)..
M.-P. Sassine, D. Mergler, R. Bowler and H.K. Hudnell, Soc. Biol. Psychiatry, 51, 909 (2002); doi:10.1016/S0006-3223(01)01350-6.
J.J. Jing and J.M. Xie, Guangdong Trace Elem. Sci., 15, 6 (2008).
M.-M. Lu, Equip. Manufact. Technol., 5, 22 (2008).
J.S. Roitz and K.W. Bruland, Anal. Chim. Acta, 344, 175 (1997); doi:10.1016/S0003-2670(97)00041-X.
J. Mierzwa, Y.-C. Sun and M.-H. Yang, Spectrochim. Acta B, 53, 63 (1998); doi:10.1016/S0584-8547(97)00119-5.
N. Tokman, J. Hazard. Mater., 143, 87 (2007); doi:10.1016/j.jhazmat.2006.08.068.
F. Sabermahani and M.A. Taher, Anal. Chim. Acta, 565, 152 (2006); doi:10.1016/j.aca.2006.02.048.