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Synthesis of Poly(methylmethacrylate-co-N-vinyl-2-pyrrolidone) Polymer
Corresponding Author(s) : Yuanhua Lin
Asian Journal of Chemistry,
Vol. 26 No. 17 (2014): Vol 26 Issue 17
Abstract
The synthesis of polymer poly(methyl methacrylate-co-N-vinyl-2-pyrrolidone) [P(MMA-co-VP)] from 2-(methoxycarbonyl)-1-propene monomer and N-vinyl-2-pyrrolidone monomer in the presence of potassium peroxidisulfate was done at 75 ºC. The polymerization was refluxed for 6 h under continuous stirring. Nitrogen gas was used to remove the oxygen present in the reflux container during the whole reaction. The polymer was further analyzed using FTIR spectroscopy, X-ray diffraction and nuclear magnetic resonance spectroscopy methods. P(MMA-co-VP) polymer also finds its application as an effective corrosion inhibitor in the presence of CO2 for J55 steel in oil and petroleum industry.
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- I. Ahamad, R. Prasad and M.A. Quraishi, Corros. Sci., 52, 933 (2010); doi:10.1016/j.corsci.2009.11.016.
- H. Gerengi and H.I. Sahin, Ind. Eng. Chem. Res., 51, 780 (2012); doi:10.1021/ie201776q.
- P.M. Krishnegowda, V.T. Venkatesha, P.K.M. Krishnegowda and S.B. Shivayogiraju, Ind. Eng. Chem. Res., 52, 722 (2013); doi:10.1021/ie3018862.
- M.A. Quraishi, A. Singh, V. Singh, D. Yadav and A.K. Singh, Mater. Chem. Phys., 122, 114 (2010); doi:10.1016/j.matchemphys.2010.02.066.
- A. Singh, I. Ahamad, V.K. Singh and M.A. Quraishi, J. Solid State Electrochem., 15, 1087 (2011); doi:10.1007/s10008-010-1172-z.
- G. Chen, M. Zhang, J. Zhao, R. Zhou, Z. Meng and J. Zhang, Chem. Cent. J., 7, 83 (2013); doi:10.1186/1752-153X-7-83.
- X.G. Li, H.Y. Wang and M.R. Huang, Macromolecules, 40, 1489 (2007); doi:10.1021/ma062463g.
- D.K. Yadav, D.S. Chauhan, I. Ahamad and M.A. Quraishi, RSC Adv., 3, 632 (2012); doi:10.1039/c2ra21697c.
- A.O. Yuce, R. Solmaz and G. Kardas, Mater. Chem. Phys., 131, 615 (2012); doi:10.1016/j.matchemphys.2011.10.026.
References
I. Ahamad, R. Prasad and M.A. Quraishi, Corros. Sci., 52, 933 (2010); doi:10.1016/j.corsci.2009.11.016.
H. Gerengi and H.I. Sahin, Ind. Eng. Chem. Res., 51, 780 (2012); doi:10.1021/ie201776q.
P.M. Krishnegowda, V.T. Venkatesha, P.K.M. Krishnegowda and S.B. Shivayogiraju, Ind. Eng. Chem. Res., 52, 722 (2013); doi:10.1021/ie3018862.
M.A. Quraishi, A. Singh, V. Singh, D. Yadav and A.K. Singh, Mater. Chem. Phys., 122, 114 (2010); doi:10.1016/j.matchemphys.2010.02.066.
A. Singh, I. Ahamad, V.K. Singh and M.A. Quraishi, J. Solid State Electrochem., 15, 1087 (2011); doi:10.1007/s10008-010-1172-z.
G. Chen, M. Zhang, J. Zhao, R. Zhou, Z. Meng and J. Zhang, Chem. Cent. J., 7, 83 (2013); doi:10.1186/1752-153X-7-83.
X.G. Li, H.Y. Wang and M.R. Huang, Macromolecules, 40, 1489 (2007); doi:10.1021/ma062463g.
D.K. Yadav, D.S. Chauhan, I. Ahamad and M.A. Quraishi, RSC Adv., 3, 632 (2012); doi:10.1039/c2ra21697c.
A.O. Yuce, R. Solmaz and G. Kardas, Mater. Chem. Phys., 131, 615 (2012); doi:10.1016/j.matchemphys.2011.10.026.