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Vol. 33 No. 5 (2021): Vol 33 Issue 5, 2021

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Synthesis and Characterization of Poly(acrylamide) Hydrogels as pH and Salt Sensitive Material

https://doi.org/10.14233/ajchem.2021.23124
Madhusudana Thippeswamy
Department of Pharmaceutical Chemistry, Kuvempu University, P.G. Centre, Kadur-577548, India
Mamatha Ganjeenahalli Puttagiddappa
Department of Chemistry, Davangere University, Shivagangotri, Davangere-577002, India
Demappa Thippaiah
Department of Polymer Science, University of Mysore, Sir M.V.P.G. Centre, Mandya-571402, India
Nayak Devappa Satyanarayan
Department of Pharmaceutical Chemistry, Kuvempu University, P.G. Centre, Kadur-577548, India

Corresponding Author(s) : Mamatha Ganjeenahalli Puttagiddappa

mamatha_gp2005@rediffmail.com; vmskt5@gmail.com

Asian Journal of Chemistry, Vol. 33 No. 5 (2021): Vol 33 Issue 5, 2021

Abstract

This work reports the synthesis of poly(acrylamide) hydrogel and its characterization. Hydrogel will be synthesized by a chemical cross-linking method using sodium metabisulfite and potassium persulphate as initiators with crosslinker methylenebisacrylamide. The synthesized hydrogels were examined by FT-IR, SEM and TGA to determine chemical interactions in the polymer network. Moreover, the swelling study explains that hydrogels swelling capacity and it depends on the concentration of the crosslinking agent. The pH, temperature and salt solutions will impact on swelling properties. In acid and base solutions, the swelling ratio order is as follows HCl < CH3COOH < HClO4 < NaOH and the swelling ratio order in salt solutions is as follows: NaCl > CaCl2 > AlCl3.

Keywords

Hydrogel Swelling pH Crosslinking agent Acrylamide
Thippeswamy, M., Ganjeenahalli Puttagiddappa, M., Thippaiah, D., & Devappa Satyanarayan, N. (2021). Synthesis and Characterization of Poly(acrylamide) Hydrogels as pH and Salt Sensitive Material. Asian Journal of Chemistry, 33(5), 1019–1024. https://doi.org/10.14233/ajchem.2021.23124
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