Synthesis and Crystal Structure of Diethyl Dithiocarbamate Tellurium
Corresponding Author(s) : YU-CHUAN ZHANG
yuchuanzhang1946@yahoo.cn
Asian Journal of Chemistry,
Vol. 21 No. 5 (2009): Vol 21 Issue 5
Abstract
Diethyl dithiocarbamate tellurium was synthesized and characterized by IR spectra, elemental analysis. and single-crystal X-ray diffraction analysis. The crystal structure of tellurium complex was determined by single-crystal X-ray. The possessing parameters: P2(1)/c, a = 15.1640(3) Å, b = 8.4055(2)Å, c = 14.7887(2)Å, α = 90º, β = 117.228(10)º, γ = 90º, V = 1676.1(6)Å3, Z = 4, Mr = 424.12, Dc = 1.681 g/cm3, μ = 2.256 mm-1, F(000) = 840, T = 296(2)K, R1 = 0.0246, wR2 = 0.0603 for 3799 reflections with I > 2σ(I).
Keywords
Diethyl dithiocarbamate tellurium
Crystal structure
QUE, M., ZHANG, Y.-C., & BING, W. (2010). Synthesis and Crystal Structure of Diethyl Dithiocarbamate Tellurium. Asian Journal of Chemistry, 21(5), 4088–4092. Retrieved from https://asianpubs.org/index.php/ajchem/article/view/17393
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