Solvothermal Synthesis of Nano-Sized Nickel Complex with 1-Methylimidazole Using Ionic Liquid
CUNYING XU
School of Materials Science and Engineering, Kunming University of Science and Technology, No. 68, Wenchang Road, 121 Main Street, Kunming 650093, P.R. China
RULAN TANG
School of Materials Science and Engineering, Kunming University of Science and Technology, No. 68, Wenchang Road, 121 Main Street, Kunming 650093, P.R. China
YAWEI LIU
School of Materials Science and Engineering, Kunming University of Science and Technology, No. 68, Wenchang Road, 121 Main Street, Kunming 650093, P.R. China
YAN LI
School of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093, P.R. China.
YIXIN HUA
School of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093, P.R. China.
Corresponding Author(s) : CUNYING XU
xucunying@gmail.com
Asian Journal of Chemistry,
Vol. 22 No. 6 (2010): Vol 22 Issue 6
One-dimensional nanostructures of nickel complex with 1-methylimidazole [Ni(C4H6N2)6(BF4)2] have been prepared via solvothermal route using ionic liquid 1-butyl-3-methylimidazolium tetrafluoroborate salt ([bmim][BF4]) as reactive medium. The complex was characterized by elemental analysis, X-ray diffraction, scanning electron microscopy (SEM), transmission electron microscopy (TEM), infrared absorption spectroscopy, Raman spectra, magnetic measurement and thermal analysis. The SEM and TEM images indicate that the complex is rodlike with diameter of about 180-530 nm and the length of 0.29-2.80 μm. The magnetic measurement exhibits that the complex shows paramagnetic behaviour and its effective magnetic moment is 2.79 B.M.
XU, C., TANG, R., LIU, Y., LI, Y., & HUA, Y. (2010). Solvothermal Synthesis of Nano-Sized Nickel Complex with 1-Methylimidazole Using Ionic Liquid. Asian Journal of Chemistry, 22(6), 4735–4743. Retrieved from https://asianpubs.org/index.php/ajchem/article/view/16826
