Alum: An Efficient Catalyst for Trimethylsilylation of Alcohols and Phenols with Hexamethyldisilazane

Xiaojuan Yang; Jinying Liang

Issue

Vol. 24 No. 1 (2012): Vol 24 Issue 1

Issue Published : 23 September 2011

Alum: An Efficient Catalyst for Trimethylsilylation of Alcohols and Phenols with Hexamethyldisilazane

Xiaojuan Yang

College of Chemistry and Chemical Engineering, Xinxiang University, Xinxiang 453003, Henan, P.R. China

Jinying Liang

School of Pharmacy, Xinxiang Medical University, Xinxiang 453003, Henan, P.R. China

Corresponding Author(s) : Xiaojuan Yang

yangxiaojuan2005@126.com

Asian Journal of Chemistry, Vol. 24 No. 1 (2012): Vol 24 Issue 1
Article Published : 30 September 2011

Abstract

A highly convenient method for the trimethylsilylation of alcohols and phenols via treatment by hexamethyldisilazane in the presence of alum as a catalyst has been developed. A wide variety of hydroxyl groups were selectively protected in CH₃CN under mild conditions.

Keywords

Alcohol Phenol Trimethylsilyl ether Alum Catalysis

(1)

Yang, X.; Liang, J. Alum: An Efficient Catalyst for Trimethylsilylation of Alcohols and Phenols With Hexamethyldisilazane. ajc 2011, 24, 228-230.

Issue

Vol. 24 No. 1 (2012): Vol 24 Issue 1

Alum: An Efficient Catalyst for Trimethylsilylation of Alcohols and Phenols with Hexamethyldisilazane

Corresponding Author(s) : Xiaojuan Yang

Abstract

Keywords

Full Article

Download Citation

Table Of Contents