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Vol. 30 No. 3 (2018): Vol 30 Issue 3

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Synthesis, Structure and Thermal Analysis of Silver Nanoparticles using Bakelite Composite

https://doi.org/10.14233/ajchem.2018.20851
Giriraj Tailor
Polymer Science Laboratory, Department of Chemistry, Mohanlal Sukhadia University, Udaipur-313 001, India
Sarvesh Kumar Shailesh
Department of Chemistry, Baddi University of Emerging Science and Technology, Baddi-173 205, India
Jyoti Chaudhary
Polymer Science Laboratory, Department of Chemistry, Mohanlal Sukhadia University, Udaipur-313 001, India
Suhail Afzal
Department of Chemistry, Baddi University of Emerging Science and Technology, Baddi-173 205, India

Corresponding Author(s) : Sarvesh Kumar Shailesh

skshailesh07@gmail.com

Asian Journal of Chemistry, Vol. 30 No. 3 (2018): Vol 30 Issue 3

Abstract

In present work, silver nanoparticles are synthesized using phenol and formaldehyde by chemical precipitation method. To obtain the silver nanoparticles, synthesized bakelite complex is decomposed at the 1100 ºC. The formation of the synthesized bakelite composite is confirmed by the infra-red spectroscopy and nuclear magnetic resonance spectroscopy. The chemical composition and crystallographic structure of silver nanoparticles are confirmed by XRD, while scanning electron microscopy and atomic force microscopy are used to characterize the morphology of nanoparticles as well as the distribution of nanoparticle in composite. The SEM analysis indicates the ductile and catastrophic brittle fracture present on the surface of the nanoparticles. The XRD analysis revealed the size of the nanoparticle and the crystal structure which are 24 nm and orthorhombic, respectively. Thermogravimetric analysis determined the 68 % stability of compound at 900 ºC and the process being endothermic.

Keywords

Bakelite Catastrophic brittle Silver nanoparticles Orthorhombic
Tailor, G., Shailesh, S. K., Chaudhary, J., & Afzal, S. (2018). Synthesis, Structure and Thermal Analysis of Silver Nanoparticles using Bakelite Composite. Asian Journal of Chemistry, 30(3), 483–486. https://doi.org/10.14233/ajchem.2018.20851
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