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Vol. 17 No. 2 (2005): Vol 17 Issue 2

Synthesis and Crystal Structure of 2,3,4-Tri-O-acetyl-b-D-xylopyranosyl Isothiocyanate

Bo Yang
College of Chemistry and Molecular Engineering, Quingdao University of Science and Technology, Qingdao 266 042, P.R. China
Shu-Sheng Zhang
College of Chemistry and Molecular Engineering, Quingdao University of Science and Technology, Qingdao 266 042, P.R. China
Ji-Zhi Li
College of Chemistry and Molecular Engineering, Quingdao University of Science and Technology, Qingdao 266 042, P.R. China
Xu-Mei Li
College of Chemistry and Molecular Engineering, Quingdao University of Science and Technology, Qingdao 266 042, P.R. China
Kui Jiao
College of Chemistry and Molecular Engineering, Quingdao University of Science and Technology, Qingdao 266 042, P.R. China

Corresponding Author(s) : Shu-Sheng Zhang

zhangshush@public.qd.sd.cn

Asian Journal of Chemistry, Vol. 17 No. 2 (2005): Vol 17 Issue 2

Abstract

The crystal structure of 2,3,4-tri-O-acetyl-b-D-xylopyranosyl isothiocyanate, C12H15NO7S, has been synthesized and its structure is determined by X-ray crystallography and TG/DTG method. The crystal belongs to triclinic system, space group PI with unit cell constants a = 7.824(3), b = 9.252(3), c = 10.827(4) Å3, Z = 1, Dc = 1.371 g/cm3, μ = 0.241 mm–1, R and wR are 0.0474 and 0.1171 respectively for 3548 unique reflections with 3018 observed reflections [I > 2s(I)]. All the ring substituents are in plane and occupy equatorial positions.

Keywords

Synthesis Crystal structure Xylopyranosyl isothiocyanate
(1)
Yang, B.; Zhang, S.-S.; Li, J.-Z.; Li, X.-M.; Jiao, K. Synthesis and Crystal Structure of 2,3,4-Tri-O-Acetyl-B-D-Xylopyranosyl Isothiocyanate. ajc 2016, 17, 1147-1154.
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