Synthesis and Crystal Structure of Ethyl 4-(4- Nitrobenzamido)-3-(N-methyl-4-nitrobenzamido)- benzoate Monohydrate
Corresponding Author(s) : SHU-SHENG ZHANG
shushzhang@126.com
Asian Journal of Chemistry,
Vol. 19 No. 5 (2007): Vol 19 Issue 5
Abstract
In this article, ethyl 4-(4-Nitrobenzamido)-3-(N-methyl-4-nitrobenzamido)benzoate monohydrate was synthesized through the reaction of 4-nitrobenzoyl chloride and 3,4-diamino benzoate using Et3N as acid acceptor. The structure of the present compound was characterized using elemental analysis, IR, 1H NMR spectra and X-ray crystallography. The compound crystallizes in the triclinic system, space group P-1, with cell dimensions of a = 7.394(6), b = 11.418(8), c = 14.293(11)Å, α = 84.132(13), β = 81.034(13), γ = 89.451(13)º, V = 1185.7(16) Å3 and Z = 2.
Keywords
4-(4-Nitrobenzamido)-3-(N-methyl-4-nitrobenzamido) benzoate monohydrate
Crystal structure
Synthesis
LI, X.-M., ZHANG, F., DU, L.-P., & ZHANG, S.-S. (2010). Synthesis and Crystal Structure of Ethyl 4-(4- Nitrobenzamido)-3-(N-methyl-4-nitrobenzamido)- benzoate Monohydrate. Asian Journal of Chemistry, 19(5), 3923–3928. Retrieved from https://asianpubs.org/index.php/ajchem/article/view/13297
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