Microwave-Assisted Synthesis of Di-sec-butyl Disulphide by Phase Transfer Catalysis under Solvent-Free Conditions

Guoqin Hu; Xiaojun Wang; Hua Li; Yadong Zhang

Issue

Vol. 22 No. 9 (2010): Vol 22 Issue 9

Issue Published : 7 July 2010

Microwave-Assisted Synthesis of Di-sec-butyl Disulphide by Phase Transfer Catalysis under Solvent-Free Conditions

Guoqin Hu

School of Chemical Engineering and Energy, Zhengzhou University, Zhengzhou, Henan, P.R. China

Xiaojun Wang

School of Chemical Engineering and Energy, Zhengzhou University, Zhengzhou, Henan, P.R. China

Hua Li

School of Chemical Engineering and Energy, Zhengzhou University, Zhengzhou, Henan, P.R. China

Yadong Zhang

School of Chemical Engineering and Energy, Zhengzhou University, Zhengzhou, Henan, P.R. China

Corresponding Author(s) : Guoqin Hu

huguoqin@zzu.edu.cn

Asian Journal of Chemistry, Vol. 22 No. 9 (2010): Vol 22 Issue 9
Article Published : 9 July 2010

Abstract

Di-sec-butyl disulphide was synthesized by phase transfer catalysis under microwave irradiation and solvent-free conditions. The optimal experiment conditions were obtained by single-factor and orthogonal designs. The samples synthesized under the optimal conditions were characterized by infrared spectrometer, ¹H-nuclear magnetic resonance and gas chromatograph.

Keywords

Microwave-assisted synthesis Solvent-free Phase transfer catalysis Sec-butyl bromide Di-sec-butyl disulphide

(1)

Hu, G.; Wang, X.; Li, H.; Zhang, Y. Microwave-Assisted Synthesis of Di-Sec-Butyl Disulphide by Phase Transfer Catalysis under Solvent-Free Conditions. ajc 2010, 22, 7213-7218.

Issue

Vol. 22 No. 9 (2010): Vol 22 Issue 9

Microwave-Assisted Synthesis of Di-sec-butyl Disulphide by Phase Transfer Catalysis under Solvent-Free Conditions

Corresponding Author(s) : Guoqin Hu

Abstract

Keywords

Full Article

Download Citation

Table Of Contents