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Vol. 29 No. 7 (2017): Vol 29 Issue 7

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Synthesis of Silver Nanoparticles by Reduction of Silver Ion with m-Hydroxybenzoic Acid

https://doi.org/10.14233/ajchem.2017.20436
Gusrizal Gusrizal
Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Gadjah Mada, Sekip Utara, PO Box BLS 21, Yogyakarta 55281, Indonesia; Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Tanjungpura, Jl. Prof. Dr. H. Hadari Nawawi, Pontianak 78124, Indonesia
Sri Juari Santosa
Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Gadjah Mada, Sekip Utara, PO Box BLS 21, Yogyakarta 55281, Indonesia
Eko Sri Kunarti
Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Gadjah Mada, Sekip Utara, PO Box BLS 21, Yogyakarta 55281, Indonesia
Bambang Rusdiarso
Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Gadjah Mada, Sekip Utara, PO Box BLS 21, Yogyakarta 55281, Indonesia

Corresponding Author(s) : Sri Juari Santosa

sjuari@ugm.ac.id

Asian Journal of Chemistry, Vol. 29 No. 7 (2017): Vol 29 Issue 7

Abstract

In this study, we demonstrated the use of m-hydroxybenzoic acid in the synthesis of stable silver nanoparticles (AgNPs). Besides working as a reducing agent, m-hydroxybenzoic acid also simultaneously played a role as a capping agent. In the synthesis of AgNPs, silver nitrate was first mixed with the pH-adjusted m-hydroxybenzoic acid solution. The mixture was then heated in a boiling water bath. The formation of AgNPs was indicated by the appearance of yellow colour usually completed in 15 min. The reducing ability of m-hydroxybenzoic acid was affected by its pH and concentration. At a mole ratio of silver nitrate and m-hydroxybenzoic acid 1:10, the reaction produced AgNPs with the average size of 19 ± 9 nm. Stability test over a period of 18 weeks showed that AgNPs were highly stable with the intensity of surface plasmon resonance peak only reduced 2.0 %. This experiment indicates the potency of AgNPs.

Keywords

Silver nanoparticles Synthesis m-Hydroxybenzoic acid
Gusrizal, G., Santosa, S. J., Kunarti, E. S., & Rusdiarso, B. (2017). Synthesis of Silver Nanoparticles by Reduction of Silver Ion with m-Hydroxybenzoic Acid. Asian Journal of Chemistry, 29(7), 1417–1422. https://doi.org/10.14233/ajchem.2017.20436
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