Improved Manufacturing Synthesis of Phosphorus Sulphochloride

Chunhua Yang; Dequn Sun*

Issue

Vol. 23 No. 5 (2011): Vol 23 Issue 5

Issue Published : 13 January 2011

Improved Manufacturing Synthesis of Phosphorus Sulphochloride

Chunhua Yang

Marine College, Shandong University at Weihai, Wenhua West Road, No. 180, Weihai 264209, P.R. China *Corresponding author: Tel/Fax: +86 631 5688537; E-mail: dequn.sun@sdu.edu.cn

Dequn Sun*

Marine College, Shandong University at Weihai, Wenhua West Road, No. 180, Weihai 264209, P.R. China *Corresponding author: Tel/Fax: +86 631 5688537; E-mail: dequn.sun@sdu.edu.cn

Asian Journal of Chemistry, Vol. 23 No. 5 (2011): Vol 23 Issue 5
Article Published : 25 January 2011

Abstract

A practical, improved manufacturing synthesis of phosphorus sulphochloride has been developed. The one-step process with continuous 67 times repeatable batches achieved 95 % overall isolated yield using n-tributylamine as catalyst.

Keywords

Phosphorus trichloride n-Tributylamine Phosphorus sulphochloride Process.

(1)

Yang, C.; Sun*, D. Improved Manufacturing Synthesis of Phosphorus Sulphochloride. ajc 2011, 23, 2112-2114.

Issue

Vol. 23 No. 5 (2011): Vol 23 Issue 5

Improved Manufacturing Synthesis of Phosphorus Sulphochloride

Abstract

Keywords

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